rac-4-methyl-2-(sec-(2,4,6-trimethylphenethyl))aniline

Base Information

Chemical Name:rac-4-methyl-2-(sec-(2,4,6-trimethylphenethyl))aniline
CAS No.:868775-21-7
Molecular Formula:C₁₈H₂₃N
Molecular Weight:253.387
Hs Code.:

Synonyms:rac-4-methyl-2-(sec-(2,4,6-trimethylphenethyl))aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-4-methyl-2-(sec-(2,4,6-trimethylphenethyl))aniline

Chemical Property:

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Technology Process of rac-4-methyl-2-(sec-(2,4,6-trimethylphenethyl))aniline

There total 1 articles about rac-4-methyl-2-(sec-(2,4,6-trimethylphenethyl))aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 769-25-5
2,4,6-trimethylstyrene

: 106-49-0,12221-03-3
p-toluidine

: 868775-21-7
rac-4-methyl-2-(sec-(2,4,6-trimethylphenethyl))aniline

Guidance literature:: trifluorormethanesulfonic acid; In xylene; at 160 ℃; for 20h;
DOI:10.1021/ol051916j

Reference yield: 78.0%

: 868775-21-7
rac-4-methyl-2-(sec-(2,4,6-trimethylphenethyl))aniline

: 82-86-0
acenaphthene quinone

: C₄₈H₄₈N₂

Guidance literature:: With acetic acid; In toluene; at 100 ℃; for 3h;
DOI:10.1021/ja0540021

Reference yield:

: 868775-21-7
rac-4-methyl-2-(sec-(2,4,6-trimethylphenethyl))aniline

: 28923-39-9
nickel(II) bromide dimethoxyethane

: 82-86-0
acenaphthene quinone

: [NiBr₂(C₁₂H₆(NC₆H₃(CH₃)CH(CH₃)C₆H₂(CH₃)3)2)]

Guidance literature:: With CH₃COOH; In not given; condensation of acenaphthenequinone with rac-4-methyl-2-(1-(2,4,6-trimethylphenyl)ethyl)aniline in the presence of CH3COOH, then react. with Ni complex; crystn.;
DOI:10.1021/ja0540021