methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-formylindol-1-yl>methyl>-3-methoxybenzoate

Base Information

Chemical Name:methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-formylindol-1-yl>methyl>-3-methoxybenzoate
CAS No.:145889-36-7
Molecular Formula:C₂₆H₃₀N₂O₅
Molecular Weight:450.535
Hs Code.:

Synonyms:methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-formylindol-1-yl>methyl>-3-methoxybenzoate

Suppliers and Price of methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-formylindol-1-yl>methyl>-3-methoxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-formylindol-1-yl>methyl>-3-methoxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-formylindol-1-yl>methyl>-3-methoxybenzoate

There total 1 articles about methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-formylindol-1-yl>methyl>-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 70264-94-7
methyl 4-(bromomethyl)-3-methoxybenzoate

: 145889-35-6
6-<(2-ethylbutyl)carbamoyl>-3-formylindole

: 145889-36-7
methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-formylindol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 18h; Ambient temperature;
DOI:10.1021/jm00055a011

Reference yield:

: 145889-36-7
methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-formylindol-1-yl>methyl>-3-methoxybenzoate

: 145889-38-9
4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / ethanol / 0.02 h / Heating

2: Et₃N / CH₂Cl₂ / 18 h / Ambient temperature

3: H₂ / 5percent Pd/C / ethyl acetate / 18 h / 2585.7 Torr

4: aq. LiOH / tetrahydrofuran; methanol / 18 h / Ambient temperature

With lithium hydroxide; sodium tetrahydroborate; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm00055a011

Reference yield:

: 145889-36-7
methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-formylindol-1-yl>methyl>-3-methoxybenzoate

: 1027548-99-7
methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / ethanol / 0.02 h / Heating

2: Et₃N / CH₂Cl₂ / 18 h / Ambient temperature

3: H₂ / 5percent Pd/C / ethyl acetate / 18 h / 2585.7 Torr

With sodium tetrahydroborate; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm00055a011