hyper-closo-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉

Base Information

Chemical Name:hyper-closo-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉
CAS No.:61081-79-6
Molecular Formula:C₃₈H₃₉B₇P₂Ru
Molecular Weight:734.422
Hs Code.:

hyper-closo-6,6-[P(C<sub>6</sub>H<sub>5</sub>)3]2-6,2,3-RuC<sub>2</sub>B<sub>7</sub>H<sub>9</sub>

Synonyms:hyper-closo-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉

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Chemical Property of hyper-closo-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉

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Technology Process of hyper-closo-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉

There total 1 articles about hyper-closo-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.5%

: 217661-36-4
(PPh₃)3RuHCl*PhMe

: Na(1,3-C₂B₇H₁₂)

: 61081-79-6
hyper-closo-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉

Guidance literature:: In diethyl ether; byproducts: H2, P(C6H5)3, NaCl; stirred overnight; inert atmosphere; ppt. filtered off, washed with diethyl ether, extd. with dichloromethane, ethanol layered on top, left standing at -15°C for 1 d, washedwith ethanol and petroleum ether, vac. dried; elem. anal.;
DOI:10.1021/ja00394a013

Reference yield: 70.0%

: 61081-79-6
hyper-closo-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉

: 26681-85-6
di(but-3-enyl)phenylphosphine

: 74108-30-8
closo-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC₂B₇H₉

Guidance literature:: In toluene; byproducts: P(C6H5)3; (N2 or Ar); P-compound added to a stirred suspn. of Ru-complex; layered with pentane; allowed to stand overnight; cooled to -15°C for 2 days; pptd.; filtered in air; washed with methanol and petroleumether; dried in vacuo; elem. anal.;
DOI:10.1021/ja00538a014

Reference yield: 69.0%

: 61081-79-6
hyper-closo-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉

: 4124-07-6
homoallyldiphenylphosphane

: 74125-57-8
closo-6,6-(but-3-enyldiphenylphosphine)2-6,2,3-RuC₂B₇H₉

Guidance literature:: In toluene; byproducts: P(C6H5)3; (N2 or Ar); P-compound added to a stirred suspn. of Ru-complex; layered with pentane; allowed to stand overnight; cooled to -15°C for 2 days; pptd.; filtered in air; washed with methanol and petroleumether; dried in vacuo; elem. anal.;
DOI:10.1021/ja00538a014