(3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxy-3-methyl-2-furanethanol

Base Information

Chemical Name:(3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxy-3-methyl-2-furanethanol
CAS No.:1141365-70-9
Molecular Formula:C₂₆H₃₈O₄Si
Molecular Weight:442.671
Hs Code.:

Synonyms:(3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxy-3-methyl-2-furanethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxy-3-methyl-2-furanethanol

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Technology Process of (3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxy-3-methyl-2-furanethanol

There total 1 articles about (3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxy-3-methyl-2-furanethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1141365-69-6
1,1-dimethylethyl (3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxy-3-methyl-2-furanacetate

: 1141365-72-1
(3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxyl-3-methyl-2-furanacetaldehyde

: 1141365-70-9
(3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxy-3-methyl-2-furanethanol

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1002/anie.200805488

Reference yield: 52.0%

: 1141365-70-9
(3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxy-3-methyl-2-furanethanol

: 1141365-72-1
(3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxyl-3-methyl-2-furanacetaldehyde

Guidance literature:: (3S,4S)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]tetrahydro-2-methoxy-3-methyl-2-furanethanol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - -30 ℃; Inert atmosphere;
DOI:10.1002/anie.200805488