diethyl (2-hydroxy-3-(4-phenyl-1H-1,2,3-triazol-1-yl)propyl)phosphonate

Base Information

Chemical Name:diethyl (2-hydroxy-3-(4-phenyl-1H-1,2,3-triazol-1-yl)propyl)phosphonate
CAS No.:1289220-62-7
Molecular Formula:C₁₅H₂₂N₃O₄P
Molecular Weight:339.331
Hs Code.:

Synonyms:diethyl (2-hydroxy-3-(4-phenyl-1H-1,2,3-triazol-1-yl)propyl)phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (2-hydroxy-3-(4-phenyl-1H-1,2,3-triazol-1-yl)propyl)phosphonate

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Technology Process of diethyl (2-hydroxy-3-(4-phenyl-1H-1,2,3-triazol-1-yl)propyl)phosphonate

There total 2 articles about diethyl (2-hydroxy-3-(4-phenyl-1H-1,2,3-triazol-1-yl)propyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7316-37-2
diethyl (oxiran-2-ylmethyl)phosphonate

: 1289220-62-7
diethyl (2-hydroxy-3-(4-phenyl-1H-1,2,3-triazol-1-yl)propyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium sulfate; sodium azide / methanol / 4 h / 65 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C

With ammonium sulfate; sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In methanol; water; tert-butyl alcohol;
DOI:10.1080/10426507.2010.494646

Reference yield:

: 1067-87-4
Diethyl allylphosphonate

: 1289220-62-7
diethyl (2-hydroxy-3-(4-phenyl-1H-1,2,3-triazol-1-yl)propyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

2: ammonium chloride; sodium azide / methanol; water / 20 °C

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / methanol; water / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; ammonium chloride; sodium L-ascorbate; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; water;
DOI:10.3390/molecules20011088

Reference yield: 90.0%

: 1289220-62-7
diethyl (2-hydroxy-3-(4-phenyl-1H-1,2,3-triazol-1-yl)propyl)phosphonate

: 1289220-84-3
2-hydroxy-3-(4-phenyl-1,2,3-triazol-1-yl)propylphosphonic acid

Guidance literature:: With trimethylsilyl bromide; In dichloromethane; at 20 ℃; for 24h; Darkness; Inert atmosphere;
DOI:10.1080/10426507.2010.494646