3-(3-BROMOPHENYL)-3-[(2,2,2-TRIFLUOROACETYL)AMINO]PROPANOIC ACID

Base Information

• Chemical Name: 3-(3-BROMOPHENYL)-3-[(2,2,2-TRIFLUOROACETYL)AMINO]PROPANOIC ACID
• CAS No.: 117291-13-1
• Molecular Formula: C₁₁H₉BrF₃NO₃
• Molecular Weight: 340.097
• Mol file: 117291-13-1.mol

Synonyms:3-(3-bromophenyl)-3-(2,2,2-trifluoroacetamido)-propanoic acid

Chemical Property of 3-(3-BROMOPHENYL)-3-[(2,2,2-TRIFLUOROACETYL)AMINO]PROPANOIC ACID

Chemical Property:

Purity/Quality:

3-(3-Bromophenyl)-3-[(2,2,2-trifluoroacetyl)amino]propanoic acid ^*data from reagent suppliers

Safty Information:

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Technology Process of 3-(3-BROMOPHENYL)-3-[(2,2,2-TRIFLUOROACETYL)AMINO]PROPANOIC ACID

There total 2 articles about 3-(3-BROMOPHENYL)-3-[(2,2,2-TRIFLUOROACETYL)AMINO]PROPANOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3-amino-3-(3-bromo-phenyl)-propionic acid (117391-50-1,275826-35-2,788153-27-5) + trifluoroacetic anhydride (407-25-0) → 3-(3-bromophenyl)-3-(2,2,2-trifluoroacetamido)-propanoic acid (117291-13-1)

Guidance literature:

at 20 ℃; for 1.5h;

Reference yield:

m-bromobenzoic aldehyde (3132-99-8) → 3-(3-bromophenyl)-3-(2,2,2-trifluoroacetamido)-propanoic acid (117291-13-1)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium acetate / ethanol / 6 h / Heating

2: trifluoroacetic acid / 0.5 h / Heating

With ammonium acetate; trifluoroacetic acid; In ethanol;

Reference yield:

3-(3-bromophenyl)-3-(2,2,2-trifluoroacetamido)-propanoic acid (117291-13-1) → 3-(3-Bromo-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride (117291-31-3)

Guidance literature:

With thionyl chloride; In benzene; for 0.5h; Heating;

upstream raw materials:

3-amino-3-(3-bromo-phenyl)-propionic acid

trifluoroacetic anhydride

m-bromobenzoic aldehyde

Downstream raw materials:

3-(3-Bromo-phenyl)-3-(2,2,2-trifluoro-acetylamino)-propionyl chloride

4-(3-Bromo-phenyl)-imidazolidin-2-one

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