(2E,6E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,6-dien-1-ol

Base Information

Chemical Name:(2E,6E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,6-dien-1-ol
CAS No.:714956-86-2
Molecular Formula:C₂₀H₃₄O
Molecular Weight:290.489
Hs Code.:

Synonyms:(2E,6E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,6-dien-1-ol

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Chemical Property of (2E,6E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,6-dien-1-ol

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Technology Process of (2E,6E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,6-dien-1-ol

There total 8 articles about (2E,6E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,6-dien-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1006607-17-5
(2E,6E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)-1-(tetrahydro-2H-pyranyloxy)-2,6-nonadiene

: 714956-86-2
(2E,6E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,6-dien-1-ol

Guidance literature:: With pyridinium p-toluenesulfonate; In ethanol; at 55 ℃; for 13h;
DOI:10.1002/ardp.200700137

Reference yield: 76.0%

: 916651-16-6
C₂₆H₃₈O₃S

: 714956-86-2
(2E,6E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,6-dien-1-ol

Guidance literature:: With lithium; ethylamine; In diethyl ether; at -78 ℃;
DOI:10.1055/s-2006-949641

Reference yield:

: 37905-04-7
(2E,6E)-8-bromo-3,7-dimethylocta-2,6-dienyl acetate

: 714956-86-2
(2E,6E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,6-dien-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: n-BuLi; HMPA / tetrahydrofuran / -78 °C

2: 76 percent / Li; EtNH₂ / diethyl ether / -78 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; lithium; ethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1055/s-2006-949641