2-(3-iodo-4-methylphenyl)-6-(4-methyl-1H-imidazol-1-yl)-1H-benzo[d]imidazole

Base Information

Chemical Name:2-(3-iodo-4-methylphenyl)-6-(4-methyl-1H-imidazol-1-yl)-1H-benzo[d]imidazole
CAS No.:1542265-56-4
Molecular Formula:C₁₈H₁₅IN₄
Molecular Weight:414.248
Hs Code.:

Synonyms:2-(3-iodo-4-methylphenyl)-6-(4-methyl-1H-imidazol-1-yl)-1H-benzo[d]imidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3-iodo-4-methylphenyl)-6-(4-methyl-1H-imidazol-1-yl)-1H-benzo[d]imidazole

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Technology Process of 2-(3-iodo-4-methylphenyl)-6-(4-methyl-1H-imidazol-1-yl)-1H-benzo[d]imidazole

There total 6 articles about 2-(3-iodo-4-methylphenyl)-6-(4-methyl-1H-imidazol-1-yl)-1H-benzo[d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.3%

: 1542265-55-3
N-(2-amino-4-(4-methyl-1H-imidazol-1-yl)phenyl)-3-iodo-4-methyl benzamide

: 1542265-56-4
2-(3-iodo-4-methylphenyl)-6-(4-methyl-1H-imidazol-1-yl)-1H-benzo[d]imidazole

Guidance literature:: In acetic acid; for 8h; Reflux;

Reference yield:

: 1542265-54-2
4-(4-methyl-1H-imidazol-1-yl)-2-nitroaniline

: 1542265-56-4
2-(3-iodo-4-methylphenyl)-6-(4-methyl-1H-imidazol-1-yl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: nickel / methanol / 7 h / 2068.65 Torr

2.1: thionyl chloride / 2 h / Reflux

2.2: 20 h / 20 °C

3.1: acetic acid / 8 h / Reflux

With thionyl chloride; nickel; In methanol; acetic acid;

Reference yield:

: 875-51-4
4-Bromo-2-nitroaniline

: 1542265-56-4
2-(3-iodo-4-methylphenyl)-6-(4-methyl-1H-imidazol-1-yl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide; 8-quinolinol; ammonia / dimethyl sulfoxide; water; ethyl acetate

2.1: nickel / methanol / 7 h / 2068.65 Torr

3.1: thionyl chloride / 2 h / Reflux

3.2: 20 h / 20 °C

4.1: acetic acid / 8 h / Reflux

With copper(l) iodide; 8-quinolinol; thionyl chloride; ammonia; nickel; In methanol; water; acetic acid; dimethyl sulfoxide; ethyl acetate;