O-(2,3-di-O-acetyl-4-O-benzyl-β-D-xylopyranosyl)-(1->4)-1,2,3-tri-O-acetyl-β-D-xylopyranose

Base Information

Chemical Name:O-(2,3-di-O-acetyl-4-O-benzyl-β-D-xylopyranosyl)-(1->4)-1,2,3-tri-O-acetyl-β-D-xylopyranose
CAS No.:78423-91-3
Molecular Formula:C₂₇H₃₄O₁₄
Molecular Weight:582.559
Hs Code.:

Synonyms:O-(2,3-di-O-acetyl-4-O-benzyl-β-D-xylopyranosyl)-(1->4)-1,2,3-tri-O-acetyl-β-D-xylopyranose

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Chemical Property of O-(2,3-di-O-acetyl-4-O-benzyl-β-D-xylopyranosyl)-(1->4)-1,2,3-tri-O-acetyl-β-D-xylopyranose

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Technology Process of O-(2,3-di-O-acetyl-4-O-benzyl-β-D-xylopyranosyl)-(1->4)-1,2,3-tri-O-acetyl-β-D-xylopyranose

There total 4 articles about O-(2,3-di-O-acetyl-4-O-benzyl-β-D-xylopyranosyl)-(1->4)-1,2,3-tri-O-acetyl-β-D-xylopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78423-89-9
1,2,3-tri-O-acetyl-4-O-benzyl-β-D-xylopyranose

: 78423-91-3
O-(2,3-di-O-acetyl-4-O-benzyl-β-D-xylopyranosyl)-(1->4)-1,2,3-tri-O-acetyl-β-D-xylopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide / CH₂Cl₂; tetrahydrofuran / 0.25 h / Ambient temperature

2: 34.7 percent / mercuric cyanide / acetonitrile / 1 h / Ambient temperature

With hydrogen bromide; mercury(II) cyanide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/S0008-6215(00)81074-5

Reference yield:

: 69984-20-9
methyl α-D-xylopyranoside 4-benzyl ether

: 78423-91-3
O-(2,3-di-O-acetyl-4-O-benzyl-β-D-xylopyranosyl)-(1->4)-1,2,3-tri-O-acetyl-β-D-xylopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: acid

2: acetylation

3: H₂ / 5percent Pd/C / methanol; acetone

4: mercuric cyanide / acetonitrile

With hydrogen; mercury(II) cyanide; palladium on activated charcoal; In methanol; acetone; acetonitrile;
DOI:10.1016/S0008-6215(00)85935-2

Reference yield:

: 78424-01-8
4-O-benzyl-D-xylose

: 78423-91-3
O-(2,3-di-O-acetyl-4-O-benzyl-β-D-xylopyranosyl)-(1->4)-1,2,3-tri-O-acetyl-β-D-xylopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: acetylation

2: H₂ / 5percent Pd/C / methanol; acetone

3: mercuric cyanide / acetonitrile

With hydrogen; mercury(II) cyanide; palladium on activated charcoal; In methanol; acetone; acetonitrile;
DOI:10.1016/S0008-6215(00)85935-2