6-But-3-enyl-1,5-dimethoxy-6-(2-methoxy-ethoxymethoxymethyl)-cyclohexa-1,4-diene

Base Information

Chemical Name:6-But-3-enyl-1,5-dimethoxy-6-(2-methoxy-ethoxymethoxymethyl)-cyclohexa-1,4-diene
CAS No.:82939-72-8
Molecular Formula:C₁₇H₂₈O₅
Molecular Weight:312.406
Hs Code.:

Synonyms:6-But-3-enyl-1,5-dimethoxy-6-(2-methoxy-ethoxymethoxymethyl)-cyclohexa-1,4-diene

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Chemical Property of 6-But-3-enyl-1,5-dimethoxy-6-(2-methoxy-ethoxymethoxymethyl)-cyclohexa-1,4-diene

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Technology Process of 6-But-3-enyl-1,5-dimethoxy-6-(2-methoxy-ethoxymethoxymethyl)-cyclohexa-1,4-diene

There total 4 articles about 6-But-3-enyl-1,5-dimethoxy-6-(2-methoxy-ethoxymethoxymethyl)-cyclohexa-1,4-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58310-18-2
1,4-dihydro-2,6-dimethoxybenzoic acid

: 82939-72-8
6-But-3-enyl-1,5-dimethoxy-6-(2-methoxy-ethoxymethoxymethyl)-cyclohexa-1,4-diene

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / K₂CO₃ / acetone / 6 h / Heating

2: 1.) (i-Pr)2NLi / 1.) THF, hexane, 0 deg C, 5 min, 2.) 0 deg C, 25 h

3: 97.3 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 1 h / Ambient temperature

4: (i-Pr)2NEt / CH₂Cl₂ / 7 h / Ambient temperature

With lithium aluminium tetrahydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; acetone;

Reference yield:

: 82939-66-0
methyl 2,6-dimethoxy-2,5-cyclohexadiene-1-carboxylate

: 82939-72-8
6-But-3-enyl-1,5-dimethoxy-6-(2-methoxy-ethoxymethoxymethyl)-cyclohexa-1,4-diene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) (i-Pr)2NLi / 1.) THF, hexane, 0 deg C, 5 min, 2.) 0 deg C, 25 h

2: 97.3 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 1 h / Ambient temperature

3: (i-Pr)2NEt / CH₂Cl₂ / 7 h / Ambient temperature

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 82939-67-1
methyl 1-(but-1-en-4-yl)-2,6-dimethoxycyclohexa-2,5-diene-1-carboxylate

: 82939-72-8
6-But-3-enyl-1,5-dimethoxy-6-(2-methoxy-ethoxymethoxymethyl)-cyclohexa-1,4-diene

Guidance literature:: Multi-step reaction with 2 steps

1: 97.3 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 1 h / Ambient temperature

2: (i-Pr)2NEt / CH₂Cl₂ / 7 h / Ambient temperature

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane;