(4R,5S)-5-(4-Methoxy-phenyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid amide

Base Information

Chemical Name:(4R,5S)-5-(4-Methoxy-phenyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid amide
CAS No.:127489-34-3
Molecular Formula:C₁₃H₁₇NO₄
Molecular Weight:251.282
Hs Code.:

Synonyms:(4R,5S)-5-(4-Methoxy-phenyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5S)-5-(4-Methoxy-phenyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid amide

Chemical Property:

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Technology Process of (4R,5S)-5-(4-Methoxy-phenyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid amide

There total 4 articles about (4R,5S)-5-(4-Methoxy-phenyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 344256-01-5
5-(4-Methoxy-phenyl)-2,2-dimethyl-[1,3]dioxolane-4-carbonitrile

: 103-82-2
phenylacetic acid

: 127489-34-3
(4R,5S)-5-(4-Methoxy-phenyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid amide

: 65-85-0,8013-63-6
benzoic acid

Guidance literature:: With potassium hydroxide; In ethanol;
DOI:10.1016/S0040-4039(01)93473-2

Reference yield:

: 33646-40-1,97070-73-0,133269-64-4,139406-83-0
(S)-4-methoxymandelonitrile

: 127489-34-3
(4R,5S)-5-(4-Methoxy-phenyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid amide

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Raney nickel

2: NaHSO₃

3: H(+)

4: KOH / ethanol

With potassium hydroxide; hydrogen; hydrogen cation; sodium hydrogensulfite; nickel; In ethanol;
DOI:10.1016/S0040-4039(01)93473-2

Reference yield:

: 34025-30-4
(S)-Hydroxy-(4-methoxy-phenyl)-acetaldehyde

: 127489-34-3
(4R,5S)-5-(4-Methoxy-phenyl)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1: NaHSO₃

2: H(+)

3: KOH / ethanol

With potassium hydroxide; hydrogen cation; sodium hydrogensulfite; In ethanol;
DOI:10.1016/S0040-4039(01)93473-2