Technology Process of C18H38N4O2S2
There total 1 articles about C18H38N4O2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 1 h / 20 °C
2: methanol; sodium methylate / 3 h / 20 °C
3: hydrazine hydrate / ethanol / 16 h / Reflux
With
methanol; sodium methylate; hydrazine hydrate;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja106486b
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diothiothreitol / N,N-dimethyl-formamide / 16 h / 20 °C
2.1: acetic acid / methanol / 2 h / 20 °C / Inert atmosphere
3.1: sodium methylate / methanol; dichloromethane / 2 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: tetrakis(actonitrile)copper(I) hexafluorophosphate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / tetrahydrofuran; methanol; dichloromethane / 16 h / 20 °C / Inert atmosphere
5.1: trifluoroacetic acid / chloroform / 0.02 h / 20 °C
With
tetrakis(actonitrile)copper(I) hexafluorophosphate; sodium methylate; acetic acid; trifluoroacetic acid; diothiothreitol; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
tetrahydrofuran; methanol; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/ja106486b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diothiothreitol / N,N-dimethyl-formamide / 16 h / 20 °C
2: acetic acid / methanol / 2 h / 20 °C / Inert atmosphere
With
acetic acid; diothiothreitol;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja106486b
