lithium (3-(benzyloxy)-2-{[(4-fluorobenzyl)amino]carbonyl}-9,9-dimethyl-4-oxo-4,6,7,9-tetrahydro-8H-pyrazino[1,2-d]pyrimidin-8-yl)acetate

Base Information

Chemical Name:lithium (3-(benzyloxy)-2-{[(4-fluorobenzyl)amino]carbonyl}-9,9-dimethyl-4-oxo-4,6,7,9-tetrahydro-8H-pyrazino[1,2-d]pyrimidin-8-yl)acetate
CAS No.:911494-51-4
Molecular Formula:C₂₆H₂₆FN₄O₅*Li
Molecular Weight:500.456
Hs Code.:

Synonyms:lithium (3-(benzyloxy)-2-{[(4-fluorobenzyl)amino]carbonyl}-9,9-dimethyl-4-oxo-4,6,7,9-tetrahydro-8H-pyrazino[1,2-d]pyrimidin-8-yl)acetate

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Chemical Property of lithium (3-(benzyloxy)-2-{[(4-fluorobenzyl)amino]carbonyl}-9,9-dimethyl-4-oxo-4,6,7,9-tetrahydro-8H-pyrazino[1,2-d]pyrimidin-8-yl)acetate

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Technology Process of lithium (3-(benzyloxy)-2-{[(4-fluorobenzyl)amino]carbonyl}-9,9-dimethyl-4-oxo-4,6,7,9-tetrahydro-8H-pyrazino[1,2-d]pyrimidin-8-yl)acetate

There total 6 articles about lithium (3-(benzyloxy)-2-{[(4-fluorobenzyl)amino]carbonyl}-9,9-dimethyl-4-oxo-4,6,7,9-tetrahydro-8H-pyrazino[1,2-d]pyrimidin-8-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 911494-50-3
methyl (3-(benzyloxy)-2-{[(4-fluorobenzyl)amino]carbonyl}-9,9-dimethyl-4-oxo-4,6,7,9-tetrahydro-8H-pyrazino[1,2-a]pyrimidin-8-yl)acetate

: 911494-51-4
lithium (3-(benzyloxy)-2-{[(4-fluorobenzyl)amino]carbonyl}-9,9-dimethyl-4-oxo-4,6,7,9-tetrahydro-8H-pyrazino[1,2-d]pyrimidin-8-yl)acetate

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water;

Reference yield:

: 100-44-7
benzyl chloride

: 911494-51-4
lithium (3-(benzyloxy)-2-{[(4-fluorobenzyl)amino]carbonyl}-9,9-dimethyl-4-oxo-4,6,7,9-tetrahydro-8H-pyrazino[1,2-d]pyrimidin-8-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 65 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 65 °C

3: lithium hydroxide / tetrahydrofuran; water

With lithium hydroxide; potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;

Reference yield:

: 911491-26-4
N-(4-fluorobenzyl)-3-hydroxy-9,9-dimethyl-4-oxo-6,7,8,9-tetrahydro-4H-pyrazino[1,2-a]pyrimidine-2-carboxamide

: 911494-51-4
lithium (3-(benzyloxy)-2-{[(4-fluorobenzyl)amino]carbonyl}-9,9-dimethyl-4-oxo-4,6,7,9-tetrahydro-8H-pyrazino[1,2-d]pyrimidin-8-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 65 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 65 °C

3: lithium hydroxide / tetrahydrofuran; water

With lithium hydroxide; potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;