2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

Base Information

• Chemical Name: 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose
• CAS No.: 1042225-09-1
• Molecular Formula: C₅₂H₄₅NO₁₈
• Molecular Weight: 971.925

Synonyms:2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

Chemical Property of 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

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Technology Process of 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

There total 1 articles about 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

4-methoxyphenyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside (1042225-08-0) → 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose (1042225-09-1)

Guidance literature:

With ceric ammonium nitrate; In water; acetonitrile; at 0 ℃; for 0.5h;

DOI:10.1039/b802235f

Reference yield: 73.0%

2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose (1042225-09-1) + trichloroacetonitrile (545-06-2) → C54H45Cl3N2O18 (1042225-10-4)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃;

DOI:10.1039/b802235f

upstream raw materials:

4-methoxyphenyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Downstream raw materials:

C₅₄H₄₅Cl₃N₂O₁₈

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