2-[((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)sulfanyl]-1H-benzimidazole

Base Information

Chemical Name:2-[((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)sulfanyl]-1H-benzimidazole
CAS No.:1355709-99-7
Molecular Formula:C₁₇H₂₄N₂S
Molecular Weight:288.457
Hs Code.:

Synonyms:2-[((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)sulfanyl]-1H-benzimidazole

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Chemical Property of 2-[((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)sulfanyl]-1H-benzimidazole

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Technology Process of 2-[((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)sulfanyl]-1H-benzimidazole

There total 2 articles about 2-[((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)sulfanyl]-1H-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 2230-82-2
menthyl tosylate

: 134469-07-1
Benzimidazol-2-thiol

: 1355709-99-7
2-[((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)sulfanyl]-1H-benzimidazole

Guidance literature:: Benzimidazol-2-thiol; With tetra-(n-butyl)ammonium iodide; caesium carbonate; In ethanol; at 20 ℃; for 1h;

menthyl tosylate; In ethanol; for 24h; Reflux;
DOI:10.1007/s10600-012-0099-2

Reference yield:

: 2230-82-2,2230-91-3,7212-65-9,14539-75-4,14539-76-5,60183-51-9,63559-37-5,2230-77-5
(1S,2S,5R)-(+)-2-isopropyl-5-methylcyclohexyl tosylate

: 134469-07-1
Benzimidazol-2-thiol

: 1355709-99-7
2-[((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)sulfanyl]-1H-benzimidazole

Guidance literature:: With tetra-(n-butyl)ammonium iodide; caesium carbonate; In ethanol; at 78 ℃;
DOI:10.1007/s10600-012-0153-0

Reference yield:

: 1355709-99-7
2-[((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)sulfanyl]-1H-benzimidazole

: 1361560-35-1
2-{(S)-[(1S,2S,5R)-2-isopropyl-5-methylcyclohexyl]sulfinyl}-1H-benzimidazole

: 1361560-33-9
2-{(R)-[(1S,2S,5R)-2-isopropyl-5-methylcyclohexyl]sulfinyl}-1H-benzimidazole

Guidance literature:: With titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide; water; In dichloromethane; at 0 ℃; for 16h; optical yield given as %de;
DOI:10.1134/S1070428012010186