4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine

Base Information

• Chemical Name: 4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine
• CAS No.: 88150-58-7
• Molecular Formula: C₂₃H₂₉ClN₂O₇
• Molecular Weight: 480.945

Synonyms:4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine

Chemical Property of 4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine

Chemical Property:

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Technology Process of 4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine

There total 1 articles about 4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

2-[(2-aminoethoxy)methyl]-4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine (88150-42-9) + bromoacetic acid methyl ester (96-32-2) → 4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine (88150-58-7) + 2-<<2-amino>ethoxy>methyl>-4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridine (123700-30-1)

Guidance literature:

With potassium carbonate; In acetonitrile; for 2h; Heating;

DOI:10.1021/jm00164a019

Reference yield: 97.0%

4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine (88150-58-7) + methyl isocyanate (624-83-9) → 1-<2-<<4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-1-<(methoxycarbonyl)methyl>-3-methylurea (93849-28-6)

Guidance literature:

In dichloromethane; for 2h; Ambient temperature;

DOI:10.1021/jm00168a041

Reference yield: 74.0%

potassium cyanate (590-28-3) + 4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine (88150-58-7) → 1-<2-<<4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-1-<(methoxycarbonyl)methyl>urea (93849-06-0)

Guidance literature:

With acetic acid; In 1,4-dioxane; water; for 1.16667h; Ambient temperature;

DOI:10.1021/jm00168a041

upstream raw materials:

2-[(2-aminoethoxy)methyl]-4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

bromoacetic acid methyl ester

Downstream raw materials:

1-<2-<<4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-1-<(methoxycarbonyl)methyl>urea

UK-51656

N-(2-aminoethyl)-2-<<2-<<4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>amino>acetamide

1-<2-<<4-(2-chlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>-1-<(methoxycarbonyl)methyl>-3-methylurea

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