diphenylsulfonium-benzoyl-Val-βAla-Phe-Gly-NH2 trifluoromethanesulfonate

Base Information

Chemical Name:diphenylsulfonium-benzoyl-Val-βAla-Phe-Gly-NH2 trifluoromethanesulfonate
CAS No.:1374560-89-0
Molecular Formula:CF₃O₃S*C₃₈H₄₂N₅O₅S
Molecular Weight:829.918
Hs Code.:

Synonyms:diphenylsulfonium-benzoyl-Val-βAla-Phe-Gly-NH2 trifluoromethanesulfonate

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Chemical Property of diphenylsulfonium-benzoyl-Val-βAla-Phe-Gly-NH2 trifluoromethanesulfonate

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Technology Process of diphenylsulfonium-benzoyl-Val-βAla-Phe-Gly-NH2 trifluoromethanesulfonate

There total 2 articles about diphenylsulfonium-benzoyl-Val-βAla-Phe-Gly-NH2 trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: C₁₉H₂₈N₅O₄Pol

: 1229186-21-3
(4-carboxyphenyl)(diphenyl)sulfonium trifluoromethanesulfonate

: 1374560-89-0
diphenylsulfonium-benzoyl-Val-βAla-Phe-Gly-NH2 trifluoromethanesulfonate

Guidance literature:: (4-carboxyphenyl)(diphenyl)sulfonium trifluoromethanesulfonate; With 4-methyl-morpholine; 4‐(4,6dimethoxy‐1,3,5‐triazin‐2‐yl)‐4‐methylmorpholinium tetrafluoroborate; In N,N-dimethyl-formamide; at 20 ℃; for 0.666667h;

C₁₉H₂₈N₅O₄Pol; In N,N-dimethyl-formamide; at 20 ℃; solid phase reaction;

With chlorotriisopropylsilane; water; trifluoroacetic acid;
DOI:10.1002/ejoc.201101730

Reference yield:

: 619-58-9
4-iodobenzoic acid

: 1374560-89-0
diphenylsulfonium-benzoyl-Val-βAla-Phe-Gly-NH2 trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.17 h / 20 °C

1.2: 3.5 h / -40 - -10 °C

2.1: 4-methyl-morpholine; 4‐(4,6dimethoxy‐1,3,5‐triazin‐2‐yl)‐4‐methylmorpholinium tetrafluoroborate / N,N-dimethyl-formamide / 0.67 h / 20 °C

2.2: 20 °C / solid phase reaction

With 4-methyl-morpholine; 4‐(4,6dimethoxy‐1,3,5‐triazin‐2‐yl)‐4‐methylmorpholinium tetrafluoroborate; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201101730