C₄₁H₅₀Br₂O₆

Base Information

Chemical Name:C₄₁H₅₀Br₂O₆
CAS No.:1447017-47-1
Molecular Formula:C₄₁H₅₀Br₂O₆
Molecular Weight:798.652
Hs Code.:

C<sub>41</sub>H<sub>50</sub>Br<sub>2</sub>O<sub>6</sub>

Synonyms:C₄₁H₅₀Br₂O₆

Suppliers and Price of C₄₁H₅₀Br₂O₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₁H₅₀Br₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₁H₅₀Br₂O₆

There total 13 articles about C₄₁H₅₀Br₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 586-76-5
4-Bromobenzoic acid

: 1447017-45-9
C₂₇H₄₄O₄

: 1447017-47-1
C₄₁H₅₀Br₂O₆

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/chem.201301186

Reference yield:

: 37772-20-6
3β,6α-diacetoxy-5α-pregn-9(11)-en-20-one

: 1447017-47-1
C₄₁H₅₀Br₂O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hydroxide / tert-butyl alcohol; water / 17 h / 30 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 2 h / -70 °C

3.1: n-butyllithium / tetrahydrofuran / 0.08 h / 20 °C

3.2: 9.5 h / -25 °C

4.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

5.1: calcium carbonate / methanol / 0.33 h / -80 °C

5.2: 0.33 h / -80 °C

6.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

With 2,6-dimethylpyridine; dmap; n-butyllithium; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; calcium carbonate; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/chem.201301186

Reference yield:

: C₃₁H₅₈O₄Si₂

: 1447017-47-1
C₄₁H₅₀Br₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: t-butyldimethylsiyl triflate; 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C

2.1: potassium tert-butylate / tetrahydrofuran / 20 °C

2.2: 4 h / 30 °C

3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 20 h / 50 °C

3.2: 1 h / 0 - 25 °C

4.1: 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 0 °C / Molecular sieve

4.2: 0 - 20 °C

5.1: perchloric acid / water / 1 h / 100 °C

6.1: potassium hydroxide / tert-butyl alcohol; water / 17 h / 30 °C

7.1: 2,6-dimethylpyridine / dichloromethane / 2 h / -70 °C

8.1: n-butyllithium / tetrahydrofuran / 0.08 h / 20 °C

8.2: 9.5 h / -25 °C

9.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

10.1: calcium carbonate / methanol / 0.33 h / -80 °C

10.2: 0.33 h / -80 °C

11.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

With 2,6-dimethylpyridine; dmap; n-butyllithium; perchloric acid; t-butyldimethylsiyl triflate; potassium tert-butylate; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; calcium carbonate; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol; 2.1: |Wittig Olefination / 2.2: |Wittig Olefination / 4.2: |Ley Oxidation;
DOI:10.1002/chem.201301186