p-dodecylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:p-dodecylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside
CAS No.:916497-94-4
Molecular Formula:C₄₀H₅₂O₆S
Molecular Weight:660.915
Hs Code.:

Synonyms:p-dodecylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

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Chemical Property of p-dodecylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

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Technology Process of p-dodecylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

There total 6 articles about p-dodecylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 916497-85-3
(2R,4aR,6R,7S,8R,8aR)-8-Benzyloxy-6-(4-dodecyl-phenylsulfanyl)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 108-24-7
acetic anhydride

: 916497-94-4
p-dodecylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: With pyridine;
DOI:10.1016/j.bmcl.2006.08.095

Reference yield:

: 916497-82-0
Acetic acid (2R,3R,4S,5S,6R)-3,5-diacetoxy-2-acetoxymethyl-6-(4-dodecyl-phenylsulfanyl)-tetrahydro-pyran-4-yl ester

: 916497-94-4
p-dodecylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / potassium hydroxide / methanol

2: 90 percent / pyridine

3: 67 percent / lithium aluminum hydride; aluminum chloride

4: 100 percent / pyridine

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; In methanol;
DOI:10.1016/j.bmcl.2006.08.095

Reference yield:

: 20025-90-5
p-dodecylbenzenethiol

: 916497-94-4
p-dodecylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / boron trifluoride diethyl etherate / CH₂Cl₂ / 12 h / 20 °C

2: 100 percent / potassium hydroxide / methanol

3: 90 percent / pyridine

4: 67 percent / lithium aluminum hydride; aluminum chloride

5: 100 percent / pyridine

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; boron trifluoride diethyl etherate; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2006.08.095