N'-1-hexanoyl-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

Base Information

• Chemical Name: N'-1-hexanoyl-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide
• CAS No.: 1024003-76-6
• Molecular Formula: C₂₁H₂₄F₂N₄O₂
• Molecular Weight: 402.444

Synonyms:N'-1-hexanoyl-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

Chemical Property of N'-1-hexanoyl-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

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Technology Process of N'-1-hexanoyl-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

There total 1 articles about N'-1-hexanoyl-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carbohydrazide (1024005-20-6) + hexanoic acid (142-62-1) → N'-1-hexanoyl-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carbohydrazide (1024003-76-6)

Guidance literature:

hexanoic acid; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 - 35 ℃; for 0.5h;

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide; In N,N-dimethyl-formamide; for 8 - 16h;

Reference yield: 95.0%

N'-1-hexanoyl-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carbohydrazide (1024003-76-6) → 2-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3yl]-5-pentyl-1,3,4-oxadiazole (1024003-80-2)

Guidance literature:

With trichlorophosphate; In toluene; for 8 - 16h; Heating / reflux;

upstream raw materials:

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

hexanoic acid

Downstream raw materials:

2-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3yl]-5-pentyl-1,3,4-oxadiazole

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