1,5-di-p-tolyl-3,7-di(5'-allyl-2'-ethoxybenzyl)-1,5,3,7-diazadiphosphacyclooctane

Base Information

Chemical Name:1,5-di-p-tolyl-3,7-di(5'-allyl-2'-ethoxybenzyl)-1,5,3,7-diazadiphosphacyclooctane
CAS No.:540469-74-7
Molecular Formula:C₄₂H₅₂N₂O₂P₂
Molecular Weight:678.835
Hs Code.:

Synonyms:1,5-di-p-tolyl-3,7-di(5'-allyl-2'-ethoxybenzyl)-1,5,3,7-diazadiphosphacyclooctane

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Chemical Property of 1,5-di-p-tolyl-3,7-di(5'-allyl-2'-ethoxybenzyl)-1,5,3,7-diazadiphosphacyclooctane

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Technology Process of 1,5-di-p-tolyl-3,7-di(5'-allyl-2'-ethoxybenzyl)-1,5,3,7-diazadiphosphacyclooctane

There total 6 articles about 1,5-di-p-tolyl-3,7-di(5'-allyl-2'-ethoxybenzyl)-1,5,3,7-diazadiphosphacyclooctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-92-8
4-(prop-2-enyl)phenol

: 540469-74-7
1,5-di-p-tolyl-3,7-di(5'-allyl-2'-ethoxybenzyl)-1,5,3,7-diazadiphosphacyclooctane

Guidance literature:: Multi-step reaction with 6 steps

1: 72 h

2: 160 °C

3: 42.8 g / 12 h / 170 °C

4: 46 percent / LiAlH₄ / diethyl ether / 24 h / 20 °C

5: Heating

6: 2.6 g / ethanol / 3 h / Heating

With lithium aluminium tetrahydride; In diethyl ether; ethanol; 1: Mannich reaction / 3: Arbuzov reaction;
DOI:10.1023/A:1023345313956

Reference yield:

: 2-diethylaminomethyl-4-allylphenol

: 540469-74-7
1,5-di-p-tolyl-3,7-di(5'-allyl-2'-ethoxybenzyl)-1,5,3,7-diazadiphosphacyclooctane

Guidance literature:: Multi-step reaction with 5 steps

1: 160 °C

2: 42.8 g / 12 h / 170 °C

3: 46 percent / LiAlH₄ / diethyl ether / 24 h / 20 °C

4: Heating

5: 2.6 g / ethanol / 3 h / Heating

With lithium aluminium tetrahydride; In diethyl ether; ethanol; 2: Arbuzov reaction;
DOI:10.1023/A:1023345313956

Reference yield:

: diethyl 5-allyl-2-ethoxybenzylphosphonate

: 540469-74-7
1,5-di-p-tolyl-3,7-di(5'-allyl-2'-ethoxybenzyl)-1,5,3,7-diazadiphosphacyclooctane

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / LiAlH₄ / diethyl ether / 24 h / 20 °C

2: Heating

3: 2.6 g / ethanol / 3 h / Heating

With lithium aluminium tetrahydride; In diethyl ether; ethanol;
DOI:10.1023/A:1023345313956