C₂₉H₃₂N₄O₆S

Base Information

• Chemical Name: C₂₉H₃₂N₄O₆S
• CAS No.: 1208988-55-9
• Molecular Formula: C₂₉H₃₂N₄O₆S
• Molecular Weight: 564.662
• Mol file: 1208988-55-9.mol

Synonyms:C₂₉H₃₂N₄O₆S

Chemical Property of C₂₉H₃₂N₄O₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₂N₄O₆S

There total 8 articles about C₂₉H₃₂N₄O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethoxyphenol (500-99-2) + C22H26N4O5S2 (1208987-84-1) → C29H32N4O6S (1208988-55-9)

Guidance literature:

In acetonitrile; at 100 ℃; Inert atmosphere;

Reference yield:

2-methylthio-4-methyl-5-iodo-6-chloropyrimidine (111079-18-6) → C29H32N4O6S (1208988-55-9)

Guidance literature:

Multi-step reaction with 5 steps

1: triethylamine / 70 °C

2: methanesulfonic acid / acetone / 25 °C / Cooling with ice

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 25 °C

4: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 1 h / 100 °C

5: acetonitrile / 100 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; methanesulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; dichloromethane; acetone; acetonitrile;

Reference yield:

C12H18IN3O3S (1208987-81-8) → C29H32N4O6S (1208988-55-9)

Guidance literature:

Multi-step reaction with 4 steps

1: methanesulfonic acid / acetone / 25 °C / Cooling with ice

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 25 °C

3: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 1 h / 100 °C

4: acetonitrile / 100 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; methanesulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; dichloromethane; acetone; acetonitrile;

upstream raw materials:

3,5-dimethoxyphenol

C₂₂H₂₆N₄O₅S₂

2-mercapto-6-methylpyrimidin-4(3H)-one

6-methyl-2-methylsulfanyl-3H-pyrimidin-4-one