(2R,3S)-2,3-(methylsulfonyloxymethyl)-1,4-bis-(3,4,5-trimethoxyphenyl)butane

Base Information

Chemical Name:(2R*,3S*)-2,3-(methylsulfonyloxymethyl)-1,4-bis-(3,4,5-trimethoxyphenyl)butane
CAS No.:115495-69-7
Molecular Formula:C₂₆H₃₈O₁₂S₂
Molecular Weight:606.713
Hs Code.:

Synonyms:(2R*,3S*)-2,3-(methylsulfonyloxymethyl)-1,4-bis-(3,4,5-trimethoxyphenyl)butane

Suppliers and Price of (2R*,3S*)-2,3-(methylsulfonyloxymethyl)-1,4-bis-(3,4,5-trimethoxyphenyl)butane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R*,3S*)-2,3-(methylsulfonyloxymethyl)-1,4-bis-(3,4,5-trimethoxyphenyl)butane

Chemical Property:

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Technology Process of (2R*,3S*)-2,3-(methylsulfonyloxymethyl)-1,4-bis-(3,4,5-trimethoxyphenyl)butane

There total 1 articles about (2R*,3S*)-2,3-(methylsulfonyloxymethyl)-1,4-bis-(3,4,5-trimethoxyphenyl)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93395-16-5,110454-78-9,115587-59-2,115587-60-5,117407-00-8,135272-24-1,147783-14-0
(3S*,4R*)-3-(3,4,5-trimethoxybenzyl)-4-(3,4,5-trimethoxybenzyl)-4,5-dihydro-2(3H)-furanone

: 115495-69-7
(2R*,3S*)-2,3-(methylsulfonyloxymethyl)-1,4-bis-(3,4,5-trimethoxyphenyl)butane

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / CaCl₂, NaBH₄ / ethanol / 0.25 h / Ambient temperature

2: 91 percent / pyridine / 0.33 h / 0 °C

With pyridine; sodium tetrahydroborate; calcium chloride; In ethanol;
DOI:10.1016/S0040-4020(01)80826-7

Reference yield: 98.0%

: 115495-69-7
(2R*,3S*)-2,3-(methylsulfonyloxymethyl)-1,4-bis-(3,4,5-trimethoxyphenyl)butane

: 50544-08-6,75597-96-5,107191-91-3,115587-61-6,72730-20-2
5,5'-(2,3-dimethylbutane-1,4-diyl)bis(1,2,3-trimethoxybenzene)

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80826-7

Reference yield:

: 115495-69-7
(2R*,3S*)-2,3-(methylsulfonyloxymethyl)-1,4-bis-(3,4,5-trimethoxyphenyl)butane

: 14335-63-8,50394-06-4,72777-68-5,90130-15-7,115587-62-7
(1α,2β,3β)-6,7,8-trimethoxy-2,3-dimethyl-1-(3,4,5-trimethoxyphenyl)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / LiBEt₃ / tetrahydrofuran / 1 h / Ambient temperature

2: 35 percent / RuO₂*2H₂O, TFA, TFAA, BF₃*Et₂O / CH₂Cl₂ / 8 h / Ambient temperature

With ruthenium(IV) oxide; boron trifluoride diethyl etherate; lithium triethylborohydride; trifluoroacetic acid; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)80826-7