5-[4-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzoylamino]-isophthaloyl dichloride

Base Information

Chemical Name:5-[4-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzoylamino]-isophthaloyl dichloride
CAS No.:857680-50-3
Molecular Formula:C₁₉H₁₀Cl₂N₂O₅
Molecular Weight:417.205
Hs Code.:

Synonyms:5-[4-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzoylamino]-isophthaloyl dichloride

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Chemical Property of 5-[4-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzoylamino]-isophthaloyl dichloride

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Technology Process of 5-[4-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzoylamino]-isophthaloyl dichloride

There total 4 articles about 5-[4-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzoylamino]-isophthaloyl dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17057-04-4
N-(4-carboxyphenyl)maleimide

: 857680-50-3
5-[4-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzoylamino]-isophthaloyl dichloride

Guidance literature:: Multi-step reaction with 3 steps

1: 0.28 g / SOCl₂ / 12 h / Heating

2: 90 percent / 4-(dimethylamino)pyridine / N,N-dimethyl-acetamide / 48 h

3: SOCl₂

With dmap; thionyl chloride; In N,N-dimethyl acetamide;
DOI:10.1021/ja050339r

Reference yield:

: 29305-46-2
4-(2,5-dioxo-2,5-dihydro-1-pyrrol-1-yl)benzoyl chloride

: 857680-50-3
5-[4-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzoylamino]-isophthaloyl dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 4-(dimethylamino)pyridine / N,N-dimethyl-acetamide / 48 h

2: SOCl₂

With dmap; thionyl chloride; In N,N-dimethyl acetamide;
DOI:10.1021/ja050339r

Reference yield:

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 857680-50-3
5-[4-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzoylamino]-isophthaloyl dichloride

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / P₂O₅ / dioxane / 18 h / Heating

2: 0.28 g / SOCl₂ / 12 h / Heating

3: 90 percent / 4-(dimethylamino)pyridine / N,N-dimethyl-acetamide / 48 h

4: SOCl₂

With dmap; thionyl chloride; phosphorus pentoxide; In 1,4-dioxane; N,N-dimethyl acetamide;
DOI:10.1021/ja050339r