1-O-(2-diazo-2-phenylacetyl)-2,3;5,6-di-O-isopropylidene-α-D-mannofuranose

Base Information

Chemical Name:1-O-(2-diazo-2-phenylacetyl)-2,3;5,6-di-O-isopropylidene-α-D-mannofuranose
CAS No.:1309857-91-7
Molecular Formula:C₂₀H₂₄N₂O₇
Molecular Weight:404.42
Hs Code.:

Synonyms:1-O-(2-diazo-2-phenylacetyl)-2,3;5,6-di-O-isopropylidene-α-D-mannofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-(2-diazo-2-phenylacetyl)-2,3;5,6-di-O-isopropylidene-α-D-mannofuranose

Chemical Property:

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Technology Process of 1-O-(2-diazo-2-phenylacetyl)-2,3;5,6-di-O-isopropylidene-α-D-mannofuranose

There total 2 articles about 1-O-(2-diazo-2-phenylacetyl)-2,3;5,6-di-O-isopropylidene-α-D-mannofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 177562-09-3
1-O-(2-phenylacetyl)-2,3;5,6-di-O-isopropylidene-α-D-mannofuranose

: 1309857-91-7
1-O-(2-diazo-2-phenylacetyl)-2,3;5,6-di-O-isopropylidene-α-D-mannofuranose

: 73014-56-9
1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-β-D-mannofuranose

: 14131-84-1
2,3:5,6-di-O-isopropylidene-α-D-mannofuranose

Guidance literature:: With 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; acetonitrile; at 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2011.03.066

Reference yield:

: 103-82-2
phenylacetic acid

: 14131-84-1
2,3:5,6-di-O-isopropylidene-α-D-mannofuranose

: 1309857-91-7
1-O-(2-diazo-2-phenylacetyl)-2,3;5,6-di-O-isopropylidene-α-D-mannofuranose

: 73014-56-9
1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-β-D-mannofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane; acetonitrile / 12 h / 20 °C / Inert atmosphere

2: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane; acetonitrile / 12 h / 20 °C

With dmap; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2011.03.066