Spiro[bicyclo[2.2.1]heptane-2,5-oxazolidin]-2-one, 1,7,7-trimethyl-, (1R,2R,4R)-

Base Information

• Chemical Name: Spiro[bicyclo[2.2.1]heptane-2,5-oxazolidin]-2-one, 1,7,7-trimethyl-, (1R,2R,4R)-
• CAS No.: 222178-77-0
• Molecular Formula: C₁₂H₁₉NO₂
• Molecular Weight: 209.288
• Mol file: 222178-77-0.mol

Synonyms:Spiro[bicyclo[2.2.1]heptane-2,5-oxazolidin]-2-one, 1,7,7-trimethyl-, (1R,2R,4R)-

Chemical Property of Spiro[bicyclo[2.2.1]heptane-2,5-oxazolidin]-2-one, 1,7,7-trimethyl-, (1R,2R,4R)-

Chemical Property:

• PSA: 38.33000
• LogP: 2.64000

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Spiro[bicyclo[2.2.1]heptane-2,5-oxazolidin]-2-one, 1,7,7-trimethyl-, (1R,2R,4R)-

There total 11 articles about Spiro[bicyclo[2.2.1]heptane-2,5-oxazolidin]-2-one, 1,7,7-trimethyl-, (1R,2R,4R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C19H30N2O4Se (222178-81-6) → C12H19NO2 (222178-77-0)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 3h; Heating;

DOI:10.1016/S0040-4020(98)01133-8

Reference yield:

C17H25NO4Se (222178-79-2) → (R)-5-methyl-2-oxotetrahydrofuran (58917-25-2) + (S)-γ-valerolactone (19041-15-7) + C12H19NO2 (222178-77-0)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 3h; Heating;

DOI:10.1016/S0040-4020(98)01133-8

Reference yield:

2-aminomethyl-2-hydroxy-1,3,3-trimethyl-[2,2,1]-bicycloheptane hydrochloride + 1,1'-carbonyldiimidazole (530-62-1) → C12H19NO2 + C12H19NO2 (222178-77-0)

Guidance literature:

In tetrahydrofuran; at 70 ℃; for 3h;

DOI:10.1021/ol0069608

upstream raw materials:

C₁₇H₂₅NO₄Se

C₁₉H₃₀N₂O₄Se

1,1'-carbonyldiimidazole

di(endo-3-camphoryl) diselenide

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