C₁₄H₁₀O₃S

Base Information

Chemical Name:C₁₄H₁₀O₃S
CAS No.:1361317-36-3
Molecular Formula:C₁₄H₁₀O₃S
Molecular Weight:258.298
Hs Code.:

C<sub>14</sub>H<sub>10</sub>O<sub>3</sub>S

Synonyms:C₁₄H₁₀O₃S

Suppliers and Price of C₁₄H₁₀O₃S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₄H₁₀O₃S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₄H₁₀O₃S

There total 1 articles about C₁₄H₁₀O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 67237-53-0
3-ethynylthiophene

: 685895-45-8
2-bromo-4,6-dihydroxy-5-methylbenzaldehyde

: 1361317-36-3
C₁₄H₁₀O₃S

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 65 ℃; for 16h; Inert atmosphere;
DOI:10.1021/co300002x

Reference yield:

: 1361317-36-3
C₁₄H₁₀O₃S

: 958848-46-9
C₂₃H₁₈O₅S

Guidance literature:: Multi-step reaction with 3 steps

1: Au(OAc)3 / 1,2-dichloro-ethane / 20 °C / Inert atmosphere

2: stabilized 2-iodoxybenzoic acid; tetrabutyl ammonium fluoride / 20 °C / Inert atmosphere

3: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere

With stabilized 2-iodoxybenzoic acid; Au(OAc)3; tetrabutyl ammonium fluoride; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/co300002x

Reference yield:

: 1361317-36-3
C₁₄H₁₀O₃S

: 958840-45-4
C₂₇H₂₅NO₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: Au(OAc)3 / 1,2-dichloro-ethane / 20 °C / Inert atmosphere

2.1: stabilized 2-iodoxybenzoic acid; tetrabutyl ammonium fluoride / 20 °C / Inert atmosphere

3.1: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere

4.1: water; acetonitrile / 8 h / 20 °C / Inert atmosphere

4.2: 0.25 h / 120 °C / Inert atmosphere

4.3: Amberlite IRC₇₆ resin / 0.25 h / 120 °C / Inert atmosphere

With stabilized 2-iodoxybenzoic acid; Au(OAc)3; tetrabutyl ammonium fluoride; In dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/co300002x