1-(di-tert-butylphosphinomethyl)-2-(di-pyridin-2-ylphosphinomethyl)benzene

Base Information

Chemical Name:1-(di-tert-butylphosphinomethyl)-2-(di-pyridin-2-ylphosphinomethyl)benzene
CAS No.:1314137-34-2
Molecular Formula:C₂₆H₃₄N₂P₂
Molecular Weight:436.517
Hs Code.:

Synonyms:1-(di-tert-butylphosphinomethyl)-2-(di-pyridin-2-ylphosphinomethyl)benzene

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Chemical Property of 1-(di-tert-butylphosphinomethyl)-2-(di-pyridin-2-ylphosphinomethyl)benzene

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Technology Process of 1-(di-tert-butylphosphinomethyl)-2-(di-pyridin-2-ylphosphinomethyl)benzene

There total 4 articles about 1-(di-tert-butylphosphinomethyl)-2-(di-pyridin-2-ylphosphinomethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1000390-24-8
di-tert-butylphosphine borane

: lithium dipyridylphosphide

: 187879-67-0
1,5-dihydro-benzo[e][1,3,2]dioxathiepine 3,3-dioxide

: 1314137-34-2
1-(di-tert-butylphosphinomethyl)-2-(di-pyridin-2-ylphosphinomethyl)benzene

Guidance literature:: di-tert-butylphosphine borane; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 0.5h;

1,5-dihydro-benzo[e][1,3,2]dioxathiepine 3,3-dioxide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.16667h;

lithium dipyridylphosphide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;

Reference yield:

: 612-14-6
phthalyl alcohol

: 1314137-34-2
1-(di-tert-butylphosphinomethyl)-2-(di-pyridin-2-ylphosphinomethyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / dichloromethane / 1.5 h / 50 °C

2.1: sodium periodate / ruthenium trichloride / dichloromethane; acetonitrile; water / 1 h / 20 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / 0 - 20 °C

3.2: 1.17 h / -78 - 20 °C

3.3: -78 - 20 °C

With sodium periodate; n-butyllithium; thionyl chloride; ruthenium trichloride; In tetrahydrofuran; hexane; dichloromethane; water; acetonitrile;

Reference yield:

: 6538-31-4
1,5-dihydro-2,4,3-benzodioxadiepin-3-oxide

: 1314137-34-2
1-(di-tert-butylphosphinomethyl)-2-(di-pyridin-2-ylphosphinomethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium periodate / ruthenium trichloride / dichloromethane; acetonitrile; water / 1 h / 20 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / 0 - 20 °C

2.2: 1.17 h / -78 - 20 °C

2.3: -78 - 20 °C

With sodium periodate; n-butyllithium; ruthenium trichloride; In tetrahydrofuran; hexane; dichloromethane; water; acetonitrile;