N-<2-(6-bromo-1,3-benzodioxol-5-yl)ethyl>-2-iodo-5,6-dimethoxybenzamide

Base Information

Chemical Name:N-<2-(6-bromo-1,3-benzodioxol-5-yl)ethyl>-2-iodo-5,6-dimethoxybenzamide
CAS No.:175293-50-2
Molecular Formula:C₁₈H₁₇BrINO₅
Molecular Weight:534.145
Hs Code.:

Synonyms:N-<2-(6-bromo-1,3-benzodioxol-5-yl)ethyl>-2-iodo-5,6-dimethoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-(6-bromo-1,3-benzodioxol-5-yl)ethyl>-2-iodo-5,6-dimethoxybenzamide

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Technology Process of N-<2-(6-bromo-1,3-benzodioxol-5-yl)ethyl>-2-iodo-5,6-dimethoxybenzamide

There total 5 articles about N-<2-(6-bromo-1,3-benzodioxol-5-yl)ethyl>-2-iodo-5,6-dimethoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 63375-82-6
2-(6-bromo-benzo[1,3]dioxol-5-yl)-ethylamine

: 130260-29-6
2,3-dimethoxy-6-iodobenzoyl chloride

: 175293-50-2
N-<2-(6-bromo-1,3-benzodioxol-5-yl)ethyl>-2-iodo-5,6-dimethoxybenzamide

Guidance literature:: With triethylamine; In tetrahydrofuran; for 12h; Ambient temperature;
DOI:10.1021/jo952113k

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 175293-50-2
N-<2-(6-bromo-1,3-benzodioxol-5-yl)ethyl>-2-iodo-5,6-dimethoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaOAc, CH₃NH₂*HCl, 2.) Zn-Hg, HCl / 1.) room temperature, 2.) MeOH

2: 78 percent / AcOH / Ambient temperature

3: 83 percent / Et₃N / tetrahydrofuran / 12 h / Ambient temperature

With hydrogenchloride; methylamine hydrochloride; sodium acetate; acetic acid; triethylamine; mercury; zinc; In tetrahydrofuran;
DOI:10.1021/jo952113k

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 175293-50-2
N-<2-(6-bromo-1,3-benzodioxol-5-yl)ethyl>-2-iodo-5,6-dimethoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Tl(OCOCF₃)3, CF₃COOH, 2.) NaI

2: SOCl₂

3: 83 percent / Et₃N / tetrahydrofuran / 12 h / Ambient temperature

With thionyl chloride; triethylamine; trifluoroacetic acid; sodium iodide; thallium(III) trifluoroacetate; In tetrahydrofuran;
DOI:10.1021/jo952113k