1,2-dihydro-61-methyl-61-(3,5-bis[(dimethylamino)methyl]-4-bromophenyl)-1,2-methano[60]fullerene

Base Information

Chemical Name:1,2-dihydro-61-methyl-61-(3,5-bis[(dimethylamino)methyl]-4-bromophenyl)-1,2-methano[60]fullerene
CAS No.:214339-85-2
Molecular Formula:C₇₄H₂₁BrN₂
Molecular Weight:1017.9
Hs Code.:

Synonyms:1,2-dihydro-61-methyl-61-(3,5-bis[(dimethylamino)methyl]-4-bromophenyl)-1,2-methano[60]fullerene

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Chemical Property of 1,2-dihydro-61-methyl-61-(3,5-bis[(dimethylamino)methyl]-4-bromophenyl)-1,2-methano[60]fullerene

Chemical Property:

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Technology Process of 1,2-dihydro-61-methyl-61-(3,5-bis[(dimethylamino)methyl]-4-bromophenyl)-1,2-methano[60]fullerene

There total 3 articles about 1,2-dihydro-61-methyl-61-(3,5-bis[(dimethylamino)methyl]-4-bromophenyl)-1,2-methano[60]fullerene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1,2-dihydro-61-methyl-61-(3,5-bis[(dimethylamino)methyl]-4-bromophenyl)-1,2-methano[60]fullerene)Pd(PPh₃)2

: 7440-05-3
palladium

: 214339-85-2
1,2-dihydro-61-methyl-61-(3,5-bis[(dimethylamino)methyl]-4-bromophenyl)-1,2-methano[60]fullerene

Guidance literature:: In benzene; byproducts: PPh3; under N2; heating benzene soln. of the complex at reflux;
DOI:10.1016/S0020-1693(01)00685-5

Reference yield:

: 99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0
fullerene-C₆₀

: 214339-81-8
[2-Bromo-3-dimethylaminomethyl-5-(1-hydrazono-ethyl)-benzyl]-dimethyl-amine

: 214339-85-2
1,2-dihydro-61-methyl-61-(3,5-bis[(dimethylamino)methyl]-4-bromophenyl)-1,2-methano[60]fullerene

Guidance literature:: With manganese(IV) oxide; potassium hydroxide; Yield given. Multistep reaction; 1.) EtOH, Et₂O; 2.) toluene, 110 degC;
DOI:10.1016/S0040-4039(98)01423-3

Reference yield:

: 99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0
fullerene-C₆₀

: 214339-81-8
[2-Bromo-3-dimethylaminomethyl-5-(1-hydrazono-ethyl)-benzyl]-dimethyl-amine

: C₇₄H₂₁BrN₂

: 214339-85-2
1,2-dihydro-61-methyl-61-(3,5-bis[(dimethylamino)methyl]-4-bromophenyl)-1,2-methano[60]fullerene

Guidance literature:: With manganese(IV) oxide; potassium hydroxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) EtOH, Et₂O; 2.) toluene;
DOI:10.1016/S0040-4039(98)01423-3