Technology Process of C29H36N2O9
There total 12 articles about C29H36N2O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 82 percent / p-toluenesulfonic acid monohydrate / 23 °C
2.1: aq. H2O2; LiOH*H2O / tetrahydrofuran / 0 - 23 °C
2.2: 91 percent / tetrabutylammonium iodide; K2CO3 / dimethylformamide / 2 h / 23 °C
3.1: ozone / methanol / -78 °C
3.2: 87 percent / dimethyl sulfide / methanol / -78 °C
4.1: 224 mg / H2 / Pd/C / methanol / 23 °C
5.1: 78 percent / 2,2,2-trifluoro-ethanol / 23 °C
6.1: 87 percent / dl-camphorsulfonic acid / methanol / 3 h / 60 °C
7.1: 88 percent / pyridine / 1 h / 23 °C
With
pyridine; lithium hydroxide; camphor-10-sulfonic acid; hydrogen; dihydrogen peroxide; toluene-4-sulfonic acid; ozone;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; 2,2,2-trifluoroethanol;
DOI:10.1021/ol701446y
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ozone / methanol / -78 °C
1.2: 87 percent / dimethyl sulfide / methanol / -78 °C
2.1: 224 mg / H2 / Pd/C / methanol / 23 °C
3.1: 78 percent / 2,2,2-trifluoro-ethanol / 23 °C
4.1: 87 percent / dl-camphorsulfonic acid / methanol / 3 h / 60 °C
5.1: 88 percent / pyridine / 1 h / 23 °C
With
pyridine; camphor-10-sulfonic acid; hydrogen; ozone;
palladium on activated charcoal;
In
methanol; 2,2,2-trifluoroethanol;
DOI:10.1021/ol701446y
