(R)-2,5,7,8-tetramethyl-2-((4R,8R)-4,8,12-trimethyltridecyl)chroman-6-yl benzoate

Base Information

• Chemical Name: (R)-2,5,7,8-tetramethyl-2-((4R,8R)-4,8,12-trimethyltridecyl)chroman-6-yl benzoate
• CAS No.: 102734-34-9
• Molecular Formula: C₃₆H₅₄O₃
• Molecular Weight: 534.823

Synonyms:(R)-2,5,7,8-tetramethyl-2-((4R,8R)-4,8,12-trimethyltridecyl)chroman-6-yl benzoate

Chemical Property of (R)-2,5,7,8-tetramethyl-2-((4R,8R)-4,8,12-trimethyltridecyl)chroman-6-yl benzoate

Chemical Property:

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Technology Process of (R)-2,5,7,8-tetramethyl-2-((4R,8R)-4,8,12-trimethyltridecyl)chroman-6-yl benzoate

There total 7 articles about (R)-2,5,7,8-tetramethyl-2-((4R,8R)-4,8,12-trimethyltridecyl)chroman-6-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-benzoyl-N-methyl-4-methylbenzenesulfonamide (10533-83-2) + Tocopherol (59-02-9,18920-62-2) → (R)-2,5,7,8-tetramethyl-2-((4R,8R)-4,8,12-trimethyltridecyl)chroman-6-yl benzoate (102734-34-9)

Guidance literature:

With potassium phosphate; In tetrahydrofuran; at 23 ℃; for 15h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.orglett.8b02323

Reference yield: 80.0%

C36H53BrO3 → (R)-2,5,7,8-tetramethyl-2-((4R,8R)-4,8,12-trimethyltridecyl)chroman-6-yl benzoate (102734-34-9)

Guidance literature:

C₃₆H₅₃BrO₃; With palladium dichloride; In water; at 20 ℃; for 0.0333333h;

With 1,1,3,3-Tetramethyldisiloxane; for 11.9667h;

DOI:10.1021/ol5037369

Reference yield: 70.0%

N-benzyl-N-(tert-butoxycarbonyl)-benzamide (85909-02-0) + Tocopherol (59-02-9,18920-62-2) → (R)-2,5,7,8-tetramethyl-2-((4R,8R)-4,8,12-trimethyltridecyl)chroman-6-yl benzoate (102734-34-9)

Guidance literature:

With sodium t-butanolate; In toluene; at 150 ℃; for 24h; Sealed tube;

DOI:10.1007/s11426-020-9883-3

upstream raw materials:

Tocopherol

dibenzoyl peroxide

ethyl vinyl ether

2,5,7,8-tetramethyl-8a-[2,5,7,8-tetramethyl-2-(4,8,12-trimethyltridecyl)chroman-6-yloxy]-2-(4,8,12-trimethyltridecyl)-3,4-dihydro-2H,8aH-chromen-6-one

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