6-O-allyl-3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

Base Information

• Chemical Name: 6-O-allyl-3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine
• CAS No.: 959982-88-8
• Molecular Formula: C₄₈H₅₅N₁₁O₁₀
• Molecular Weight: 946.032

Synonyms:6-O-allyl-3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

Chemical Property of 6-O-allyl-3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 6-O-allyl-3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

There total 1 articles about 6-O-allyl-3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine + allyl bromide (106-95-6) → 6-O-allyl-3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine (959982-88-8)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃;

DOI:10.1016/j.bmc.2007.08.059

Reference yield: 64.0%

6-O-allyl-3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine (959982-88-8) + acetic anhydride (108-24-7) → 5-O-acetyl-6-O-allyl-3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmc.2007.08.059

Reference yield:

6-O-allyl-3',4'-di-O-benzyl-1-N-[(S)-2-benzyloxy-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine (959982-88-8) + 4-azido-2,3-di-O-acetyl-4,6-dideoxy-α-D-glucopyranosyl trichloroacetimidate (485809-80-1) → C58H68N14O15

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; for 5h; cooling;

DOI:10.1016/j.bmc.2007.08.059

upstream raw materials:

allyl bromide

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