1-(3,4-Dimethoxy-benzyl)-3-fluoro-5-p-tolylsulfanyl-1H-[1,2,4]triazole

Base Information

Chemical Name:1-(3,4-Dimethoxy-benzyl)-3-fluoro-5-p-tolylsulfanyl-1H-[1,2,4]triazole
CAS No.:214540-54-2
Molecular Formula:C₁₈H₁₈FN₃O₂S
Molecular Weight:359.424
Hs Code.:

Synonyms:1-(3,4-Dimethoxy-benzyl)-3-fluoro-5-p-tolylsulfanyl-1H-[1,2,4]triazole

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Chemical Property of 1-(3,4-Dimethoxy-benzyl)-3-fluoro-5-p-tolylsulfanyl-1H-[1,2,4]triazole

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Technology Process of 1-(3,4-Dimethoxy-benzyl)-3-fluoro-5-p-tolylsulfanyl-1H-[1,2,4]triazole

There total 2 articles about 1-(3,4-Dimethoxy-benzyl)-3-fluoro-5-p-tolylsulfanyl-1H-[1,2,4]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 106-45-6
para-thiocresol

: 214540-50-8
5-Bromo-1-(3,4-dimethoxy-benzyl)-3-fluoro-1H-[1,2,4]triazole

: 214540-54-2
1-(3,4-Dimethoxy-benzyl)-3-fluoro-5-p-tolylsulfanyl-1H-[1,2,4]triazole

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 23 ℃; for 12h;
DOI:10.1055/s-1998-6080

Reference yield:

: 21852-32-4
4-bromomethyl-1,2-dimethoxybenzene

: 214540-54-2
1-(3,4-Dimethoxy-benzyl)-3-fluoro-5-p-tolylsulfanyl-1H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 54.3 percent Chromat_. / NaH / dimethylformamide / 1.) -5 deg C, 30 min, 2.) 23 deg C, 12 h

2: 93 percent / K₂CO₃ / dimethylformamide / 12 h / 23 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1055/s-1998-6080

Reference yield: 43.0%

: 214540-54-2
1-(3,4-Dimethoxy-benzyl)-3-fluoro-5-p-tolylsulfanyl-1H-[1,2,4]triazole

: 1-(3,4-Dimethoxy-benzyl)-3-fluoro-1H-[1,2,4]triazole

Guidance literature:: With sodium tetrahydroborate; nickel dichloride; In tetrahydrofuran; methanol; 1.) ice-cooling, 15 min, 2.) 23 deg C, 1 h;
DOI:10.1055/s-1998-6080