2-(2-benzyl-5-chloro-1H-benzo[d]imidazol-1-yl)-N-(4-methoxybenzyl)acetamide

Base Information

Chemical Name:2-(2-benzyl-5-chloro-1H-benzo[d]imidazol-1-yl)-N-(4-methoxybenzyl)acetamide
CAS No.:1433783-14-2
Molecular Formula:C₂₄H₂₂ClN₃O₂
Molecular Weight:419.911
Hs Code.:

Synonyms:2-(2-benzyl-5-chloro-1H-benzo[d]imidazol-1-yl)-N-(4-methoxybenzyl)acetamide

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Chemical Property of 2-(2-benzyl-5-chloro-1H-benzo[d]imidazol-1-yl)-N-(4-methoxybenzyl)acetamide

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Technology Process of 2-(2-benzyl-5-chloro-1H-benzo[d]imidazol-1-yl)-N-(4-methoxybenzyl)acetamide

There total 4 articles about 2-(2-benzyl-5-chloro-1H-benzo[d]imidazol-1-yl)-N-(4-methoxybenzyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₂ClN₃O₅

: 1433783-14-2
2-(2-benzyl-5-chloro-1H-benzo[d]imidazol-1-yl)-N-(4-methoxybenzyl)acetamide

Guidance literature:: With trifluoroacetic acid; In 1,2-dichloro-ethane; at 130 ℃; for 0.333333h; Microwave irradiation;
DOI:10.1039/c3ob27404g

Reference yield:

: 103-82-2
phenylacetic acid

: 1433783-14-2
2-(2-benzyl-5-chloro-1H-benzo[d]imidazol-1-yl)-N-(4-methoxybenzyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 0.25 h / 80 °C / Microwave irradiation

2: trifluoroacetic acid / 1,2-dichloro-ethane / 0.33 h / 130 °C / Microwave irradiation

With trifluoroacetic acid; In methanol; 1,2-dichloro-ethane; 1: |Ugi Condensation;
DOI:10.1039/c3ob27404g

Reference yield:

: 954238-88-1
(2-amino-5-chlorophenyl)carbamate tert-butyl ester

: 1433783-14-2
2-(2-benzyl-5-chloro-1H-benzo[d]imidazol-1-yl)-N-(4-methoxybenzyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 0.25 h / 80 °C / Microwave irradiation

2: trifluoroacetic acid / 1,2-dichloro-ethane / 0.33 h / 130 °C / Microwave irradiation

With trifluoroacetic acid; In methanol; 1,2-dichloro-ethane; 1: |Ugi Condensation;
DOI:10.1039/c3ob27404g