(E)-(R)-7-(tert-Butyl-diphenyl-silanyloxy)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-hept-2-en-1-ol

Base Information

Chemical Name:(E)-(R)-7-(tert-Butyl-diphenyl-silanyloxy)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-hept-2-en-1-ol
CAS No.:920749-67-3
Molecular Formula:C₃₃H₅₀O₂Si
Molecular Weight:506.844
Hs Code.:

Synonyms:(E)-(R)-7-(tert-Butyl-diphenyl-silanyloxy)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-hept-2-en-1-ol

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Chemical Property of (E)-(R)-7-(tert-Butyl-diphenyl-silanyloxy)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-hept-2-en-1-ol

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Technology Process of (E)-(R)-7-(tert-Butyl-diphenyl-silanyloxy)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-hept-2-en-1-ol

There total 2 articles about (E)-(R)-7-(tert-Butyl-diphenyl-silanyloxy)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-hept-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 80434-59-9,485843-44-5,796865-68-4
(1R,2S,5R)-2-isopropyl-5-methylcyclohexanecarboxaldehyde

: 371172-65-5
(E)-tert-butyl(6-iodohex-5-en-1-yloxy)diphenylsilane

: 920749-67-3
(E)-(R)-7-(tert-Butyl-diphenyl-silanyloxy)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-hept-2-en-1-ol

Guidance literature:: (E)-tert-butyl(6-iodohex-5-en-1-yloxy)diphenylsilane; With n-butyllithium; In diethyl ether; Petroleum ether; at -78 - 20 ℃; for 1h;

(1R,2S,5R)-2-isopropyl-5-methylcyclohexanecarboxaldehyde; With trimethylaluminum; In diethyl ether; Petroleum ether; at -78 - 20 ℃;
DOI:10.1016/j.jorganchem.2006.07.028

Reference yield: 45.0%

: 80434-59-9,485843-44-5,796865-68-4
(1R,2S,5R)-2-isopropyl-5-methylcyclohexanecarboxaldehyde

: 371172-65-5
(E)-tert-butyl(6-iodohex-5-en-1-yloxy)diphenylsilane

: 920749-67-3
(E)-(R)-7-(tert-Butyl-diphenyl-silanyloxy)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-hept-2-en-1-ol

: 1042908-52-0
C₃₃H₅₀O₂Si

Guidance literature:: (E)-tert-butyl(6-iodohex-5-en-1-yloxy)diphenylsilane; With tert.-butyl lithium; In diethyl ether; hexane; at -78 - 20 ℃;

(1R,2S,5R)-2-isopropyl-5-methylcyclohexanecarboxaldehyde; With trimethylaluminum; In diethyl ether; hexane; at -78 - 20 ℃; Further stages.;
DOI:10.1021/jo800817p

Reference yield: 98.0%

: 920749-67-3
(E)-(R)-7-(tert-Butyl-diphenyl-silanyloxy)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-hept-2-en-1-ol

: 920749-70-8
[(E)-(S)-5-Azido-7-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-hept-6-enyloxy]-tert-butyl-diphenyl-silane

Guidance literature:: With hydrogen azide; triphenylphosphine; diethylazodicarboxylate; In benzene; at 0 - 20 ℃; for 6h;
DOI:10.1016/j.jorganchem.2006.07.028