((2S,3R,4R,5S,6R)-2-Benzyloxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-carbamic acid vinyl ester

Base Information

Chemical Name:((2S,3R,4R,5S,6R)-2-Benzyloxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-carbamic acid vinyl ester
CAS No.:791064-18-1
Molecular Formula:C₁₆H₂₁NO₇
Molecular Weight:339.345
Hs Code.:

Synonyms:((2S,3R,4R,5S,6R)-2-Benzyloxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-carbamic acid vinyl ester

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Chemical Property of ((2S,3R,4R,5S,6R)-2-Benzyloxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-carbamic acid vinyl ester

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Technology Process of ((2S,3R,4R,5S,6R)-2-Benzyloxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-carbamic acid vinyl ester

There total 1 articles about ((2S,3R,4R,5S,6R)-2-Benzyloxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-carbamic acid vinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 22314-39-2,22314-40-5,35812-81-8,50692-69-8,738518-26-8
phenylmethyl 2-amino-2-deoxy-α-D-glucopyranoside

: 5130-24-5
Vinyl chloroformate

: 791064-18-1
((2S,3R,4R,5S,6R)-2-Benzyloxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-carbamic acid vinyl ester

Guidance literature:: With sodium hydroxide; In phosphate buffer; at 0 ℃; for 5h; pH=8.0;
DOI:10.1021/ja049437n

Reference yield: 83.0%

: 139705-38-7
acetone O-<(vinyloxy)carbonyl>oxime

: 791064-18-1
((2S,3R,4R,5S,6R)-2-Benzyloxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-carbamic acid vinyl ester

: 791064-23-8
Carbonic acid (2R,3S,4R,5R,6S)-6-benzyloxy-3,4-dihydroxy-5-vinyloxycarbonylamino-tetrahydro-pyran-2-ylmethyl ester vinyl ester

Guidance literature:: With Candida antarctica lipase B; In tetrahydrofuran; at 45 ℃;
DOI:10.1021/ja049437n

Reference yield:

: 791064-18-1
((2S,3R,4R,5S,6R)-2-Benzyloxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-carbamic acid vinyl ester

: {3-[4-(3-Amino-propylamino)-butylamino]-propyl}-carbamic acid (2R,3S,4R,5R,6S)-5-(3-{3-[4-(3-amino-propylamino)-butylamino]-propyl}-ureido)-6-benzyloxy-3,4-dihydroxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / Candida antarctica lipase B / tetrahydrofuran / 45 °C

2: ethanol / 96 h / 45 °C

With Candida antarctica lipase B; In tetrahydrofuran; ethanol;
DOI:10.1021/ja049437n