2-anilino-N-(4-chlorophenyl)-2-oxoethanehydrazonoyl chloride

Base Information

• Chemical Name: 2-anilino-N-(4-chlorophenyl)-2-oxoethanehydrazonoyl chloride
• CAS No.: 33101-97-2
• Molecular Formula: C14H11 Cl2 N3 O
• Molecular Weight: 308.167
• Hs Code.: 2928000090
• DSSTox Substance ID: DTXSID10375695
• Mol file: 33101-97-2.mol

Synonyms:2-anilino-N-(4-chlorophenyl)-2-oxoethanehydrazonoyl chloride;33101-97-2;2-Chloro-2-[2-(4-chlorophenyl)hydrazono]-N-phenylacetamide;(1Z)-2-anilino-N-(4-chlorophenyl)-2-oxoethanehydrazonoyl chloride;DTXSID10375695;FT-0639081;(E)-N'-(4-chlorophenyl)-2-oxo-2-(phenylamino)acetohydrazonoyl chloride

Chemical Property of 2-anilino-N-(4-chlorophenyl)-2-oxoethanehydrazonoyl chloride

Chemical Property:

• Refractive Index: 1.62
• PSA: 53.49000
• Density: 1.33g/cm³
• LogP: 4.08890
• XLogP3: 5.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 307.0279174
• Heavy Atom Count: 20
• Complexity: 348

Purity/Quality:

97% ^*data from raw suppliers

N'-(4-Chlorophenyl)-2-oxo-2-(phenylamino)acetohydrazonoylchloride 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)NC(=O)C(=NNC2=CC=C(C=C2)Cl)Cl

Technology Process of 2-anilino-N-(4-chlorophenyl)-2-oxoethanehydrazonoyl chloride

There total 2 articles about 2-anilino-N-(4-chlorophenyl)-2-oxoethanehydrazonoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

4-chloro-aniline (106-47-8) + N-chloroacetyl-aniline (587-65-5) → 2-anilino-N-(4-chlorophenyl)-2-oxoethanehydrazonoyl chloride (33101-97-2)

Guidance literature:

With hydrogenchloride; sodium acetate; sodium nitrite; In ethanol; water; at 0 ℃; for 0.833333h;

DOI:10.1016/j.lfs.2022.120380

Reference yield:

→ 2-anilino-N-(4-chlorophenyl)-2-oxoethanehydrazonoyl chloride (33101-97-2)

Guidance literature:

DOI:10.1016/S0040-4020(01)90753-7

Reference yield: 85.0%

1,3-dimethyl-8-chloroxanthine (85-18-7) + 2-anilino-N-(4-chlorophenyl)-2-oxoethanehydrazonoyl chloride (33101-97-2) → 1,3-dimethyl-2,4-dioxo-6-phenylcarbamoyl-8-(p-chlorophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine

Guidance literature:

With triethylamine; In 1,4-dioxane; Heating;

DOI:10.1021/jo001626a

upstream raw materials:

4-chloro-aniline

N-chloroacetyl-aniline

Downstream raw materials:

4-(4-Chloro-phenyl)-5-imino-4,5-dihydro-[1,3,4]thiadiazole-2-carboxylic acid phenylamide

4-(4-Chloro-phenyl)-5-imino-4,5-dihydro-[1,3,4]selenadiazole-2-carboxylic acid phenylamide

2-[(4-Chloro-phenyl)-hydrazono]-2-(3,5-diamino-4-phenylazo-pyrazol-1-yl)-N-phenyl-acetamide

C₁₄H₁₁ClN₆O

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