n-octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-anhydro-α-D-lyxofuranoside

Base Information

Chemical Name:n-octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-anhydro-α-D-lyxofuranoside
CAS No.:352438-40-5
Molecular Formula:C₃₉H₄₄O₁₁
Molecular Weight:688.772
Hs Code.:

Synonyms:n-octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-anhydro-α-D-lyxofuranoside

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Chemical Property of n-octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-anhydro-α-D-lyxofuranoside

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Technology Process of n-octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-anhydro-α-D-lyxofuranoside

There total 4 articles about n-octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-anhydro-α-D-lyxofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 352438-37-0
n-octyl 2,3-anhydro-α-D-lyxofuranoside

: 352438-38-1
p-tolyl 2,3,5-tri-O-benzoyl-1-thio-α-D-arabinofuranoside

: 352438-40-5
n-octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-anhydro-α-D-lyxofuranoside

Guidance literature:: With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/jo001747a

Reference yield:

: 352438-36-9
octyl α-D-arabinofranose tetraacetate

: 352438-40-5
n-octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-anhydro-α-D-lyxofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / triphenylphosphine; diisopropylazodicarboxylate / tetrahydrofuran / 0.5 h / 0 - 20 °C

2: 91 percent / NaOMe / methanol / 4 h / 20 °C

3: 81 percent / N-iodosuccinimide; silfer triflate / CH₂Cl₂ / 0.5 h / 0 °C

With N-iodo-succinimide; di-isopropyl azodicarboxylate; sodium methylate; silver trifluoromethanesulfonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; 1: Mitsunobu reaction;
DOI:10.1021/jo001747a

Reference yield:

: 352438-08-5
n-octyl 2,3-anhydro-5-O-benzoyl-α-D-lyxofuranoside

: 352438-40-5
n-octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-anhydro-α-D-lyxofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaOMe / methanol / 4 h / 20 °C

2: 81 percent / N-iodosuccinimide; silfer triflate / CH₂Cl₂ / 0.5 h / 0 °C

With N-iodo-succinimide; sodium methylate; silver trifluoromethanesulfonate; In methanol; dichloromethane;
DOI:10.1021/jo001747a