Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC₆H₄C₅H₄NCH₃)PF₆

Base Information

Chemical Name:Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC₆H₄C₅H₄NCH₃)PF₆
CAS No.:144018-74-6
Molecular Formula:C₂₇H₃₃BClMoN₈O₂*F₆P
Molecular Weight:788.78
Hs Code.:

Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC<sub>6</sub>H<sub>4</sub>C<sub>5</sub>H<sub>4</sub>NCH<sub>3</sub>)PF<sub>6</sub>

Synonyms:Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC₆H₄C₅H₄NCH₃)PF₆

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Chemical Property of Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC₆H₄C₅H₄NCH₃)PF₆

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Technology Process of Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC₆H₄C₅H₄NCH₃)PF₆

There total 2 articles about Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC₆H₄C₅H₄NCH₃)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 144018-72-4
Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC₆H₄C₅H₄N)

: 144018-74-6
Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC₆H₄C₅H₄NCH₃)PF₆

Guidance literature:: With CH₃I; In dichloromethane; (N2), refluxed for 18 h; elem. anal.;

Reference yield:

: 17084-13-8
potassium hexafluorophosphate

: 144018-72-4
Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC₆H₄C₅H₄N)

: 144018-74-6
Cl(NO)(hydrotris(3,5-dimethylpyrazolyl)borate)molybdenum(OC₆H₄C₅H₄NCH₃)PF₆

Guidance literature:: With CH₃I; In dichloromethane; refluxing for 18 h; removal of solvent in vac.; dissolving in CH3CN; chromy. (alumina, CH3CN/aq. KPF6, room temp.); addn. of satd. aq. KPF6 to the major fraction; evapn. to dryness; extn. by partitioning between water and CH2Cl2; pptn. from the dried, concd. CH2Cl2 soln. by addn. of pentane; elem. anal.;