N-(5-chloro-2-methoxyphenyl)-3,5-bis(trifluoromethyl)benzene carbohydrazonamide

Base Information

Chemical Name:N-(5-chloro-2-methoxyphenyl)-3,5-bis(trifluoromethyl)benzene carbohydrazonamide
CAS No.:202822-41-1
Molecular Formula:C₁₆H₁₂ClF₆N₃O
Molecular Weight:411.734
Hs Code.:

Synonyms:N-(5-chloro-2-methoxyphenyl)-3,5-bis(trifluoromethyl)benzene carbohydrazonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(5-chloro-2-methoxyphenyl)-3,5-bis(trifluoromethyl)benzene carbohydrazonamide

Chemical Property:

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Technology Process of N-(5-chloro-2-methoxyphenyl)-3,5-bis(trifluoromethyl)benzene carbohydrazonamide

There total 4 articles about N-(5-chloro-2-methoxyphenyl)-3,5-bis(trifluoromethyl)benzene carbohydrazonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 202822-34-2
N-(5-chloro-2-methoxyphenyl)-3,5-bis(trifluoromethyl)benzamide

: 202822-41-1
N-(5-chloro-2-methoxyphenyl)-3,5-bis(trifluoromethyl)benzene carbohydrazonamide

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅ / benzene / 3 h / Heating

2: hydrazine / tetrahydrofuran / 1 h / 24 °C

With phosphorus pentachloride; hydrazine; In tetrahydrofuran; benzene;
DOI:10.1021/jm010569q

Reference yield:

: N-(5-chloro-2-methoxy-phenyl)-3,5-bis-trifluoromethyl-benzimidoyl chloride

: 202822-41-1
N-(5-chloro-2-methoxyphenyl)-3,5-bis(trifluoromethyl)benzene carbohydrazonamide

Guidance literature:: With hydrazine; In tetrahydrofuran; at 24 ℃; for 1h;
DOI:10.1021/jm010569q

Reference yield:

: 785-56-8
3,5-bis(trifluoromethyl)phenyl carboxylic acid chloride

: 202822-41-1
N-(5-chloro-2-methoxyphenyl)-3,5-bis(trifluoromethyl)benzene carbohydrazonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / triethylamine / tetrahydrofuran / 18 h / 24 °C

2: PCl₅ / benzene / 3 h / Heating

3: hydrazine / tetrahydrofuran / 1 h / 24 °C

With phosphorus pentachloride; triethylamine; hydrazine; In tetrahydrofuran; benzene;
DOI:10.1021/jm010569q