N-(2-Chloro-4-nitrophenyl)hydrazinecarbothioamide

Base Information

Chemical Name:N-(2-Chloro-4-nitrophenyl)hydrazinecarbothioamide
CAS No.:73305-14-3
Molecular Formula:C₇H₇ClN₄O₂S
Molecular Weight:246.677
Hs Code.:
ChEMBL ID:CHEMBL3286610
DSSTox Substance ID:DTXSID501232130

Synonyms:CHEMBL3286610;N-(2-Chloro-4-nitrophenyl)hydrazinecarbothioamide;DTXSID501232130;BDBM50019781;73305-14-3

Suppliers and Price of N-(2-Chloro-4-nitrophenyl)hydrazinecarbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-Chloro-4-nitrophenyl)hydrazinecarbothioamide

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:245.9978243
Heavy Atom Count:15
Complexity:260

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C=C1[N+](=O)[O-])Cl)NC(=S)NN

Technology Process of N-(2-Chloro-4-nitrophenyl)hydrazinecarbothioamide

There total 1 articles about N-(2-Chloro-4-nitrophenyl)hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 23165-64-2
2-chloro-4-nitrophenyl isothiocyanate

: 73305-14-3
4-(2-chloro-4-nitrophenyl)-3-thiosemicarbazide

Guidance literature:: With hydrazine hydrate; In isopropyl alcohol; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.05.044

Reference yield:

: 73305-14-3
4-(2-chloro-4-nitrophenyl)-3-thiosemicarbazide

: C₁₄H₆Cl₂N₁₀O₄S₂

Guidance literature:: Multi-step reaction with 3 steps

1: HNO₂

2: aq. NaOH

3: 68.9 percent / bromine / ethanol

With sodium hydroxide; bromine; cis-nitrous acid; In ethanol;

Reference yield:

: 73305-14-3
4-(2-chloro-4-nitrophenyl)-3-thiosemicarbazide

: 73311-09-8
(2-chloro-4-nitro-phenyl)-(5-ethylsulfanyl-[1,3,4]thiadiazol-2-yl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / Heating

2: K₂CO₃ / acetone / Heating

With potassium carbonate; In ethanol; acetone;