(S*,Z)-4-(2-(N-p-toluenesulfonamido)ethylidene)-2-ethoxytetrahydrofuran

Base Information

Chemical Name:(S*,Z)-4-(2-(N-p-toluenesulfonamido)ethylidene)-2-ethoxytetrahydrofuran
CAS No.:1416505-58-2
Molecular Formula:C₁₅H₂₁NO₄S
Molecular Weight:311.402
Hs Code.:

Synonyms:(S*,Z)-4-(2-(N-p-toluenesulfonamido)ethylidene)-2-ethoxytetrahydrofuran

Suppliers and Price of (S*,Z)-4-(2-(N-p-toluenesulfonamido)ethylidene)-2-ethoxytetrahydrofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S*,Z)-4-(2-(N-p-toluenesulfonamido)ethylidene)-2-ethoxytetrahydrofuran

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Technology Process of (S*,Z)-4-(2-(N-p-toluenesulfonamido)ethylidene)-2-ethoxytetrahydrofuran

There total 2 articles about (S*,Z)-4-(2-(N-p-toluenesulfonamido)ethylidene)-2-ethoxytetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 144-86-5
N-chloro-4-methylbenzenesulfonamide

: ((1S*,2S*)-2-ethoxy-1-vinylcyclopropyl)methanol

: 1416505-58-2
(S*,Z)-4-(2-(N-p-toluenesulfonamido)ethylidene)-2-ethoxytetrahydrofuran

Guidance literature:: With phenyltrimethylammonium tribromide; In acetonitrile; at 20 ℃; for 3h; diastereoselective reaction;
DOI:10.1021/jo302204k

Reference yield:

: 139955-11-6,140928-50-3
Methyl (E)-1-ethenyl-2-ethoxycyclopropane-1-carboxylate

: 1416505-58-2
(S*,Z)-4-(2-(N-p-toluenesulfonamido)ethylidene)-2-ethoxytetrahydrofuran

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C

2: phenyltrimethylammonium tribromide / acetonitrile / 3 h / 20 °C

With lithium aluminium tetrahydride; phenyltrimethylammonium tribromide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo302204k