Technology Process of C18H20O5
There total 12 articles about C18H20O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: Inert atmosphere
2: n-butyllithium / Inert atmosphere
3: hydrogenchloride / ethanol; water / Inert atmosphere
4: acetic acid / Inert atmosphere
5: potassium carbonate / Inert atmosphere
6: potassium tert-butylate / Inert atmosphere
7: AD-mix-β; water / Inert atmosphere
8: triethylamine / Inert atmosphere
9: sodium hydride / Inert atmosphere
10: triethylsilane; dichloro-acetic acid / Inert atmosphere
With
hydrogenchloride; triethylsilane; dichloro-acetic acid; n-butyllithium; AD-mix-β; potassium tert-butylate; water; sodium hydride; potassium carbonate; acetic acid; triethylamine;
In
ethanol; water;
4: Duff reaction / 7: Sharpless dihydroxylation;
DOI:10.1016/j.tet.2011.04.094
- Guidance literature:
-
Multi-step reaction with 8 steps
1: hydrogenchloride / ethanol; water / Inert atmosphere
2: acetic acid / Inert atmosphere
3: potassium carbonate / Inert atmosphere
4: potassium tert-butylate / Inert atmosphere
5: AD-mix-β; water / Inert atmosphere
6: triethylamine / Inert atmosphere
7: sodium hydride / Inert atmosphere
8: triethylsilane; dichloro-acetic acid / Inert atmosphere
With
hydrogenchloride; triethylsilane; dichloro-acetic acid; AD-mix-β; potassium tert-butylate; water; sodium hydride; potassium carbonate; acetic acid; triethylamine;
In
ethanol; water;
2: Duff reaction / 5: Sharpless dihydroxylation;
DOI:10.1016/j.tet.2011.04.094
