C₅₁H₇₈O₁₀Si

Base Information

Chemical Name:C₅₁H₇₈O₁₀Si
CAS No.:1448230-77-0
Molecular Formula:C₅₁H₇₈O₁₀Si
Molecular Weight:879.26
Hs Code.:

C<sub>51</sub>H<sub>78</sub>O<sub>10</sub>Si

Synonyms:C₅₁H₇₈O₁₀Si

Suppliers and Price of C₅₁H₇₈O₁₀Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₁H₇₈O₁₀Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₁H₇₈O₁₀Si

There total 16 articles about C₅₁H₇₈O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1448230-76-9
C₆₁H₈₅NO₁₂Si

: 1448230-77-0
C₅₁H₇₈O₁₀Si

Guidance literature:: With lithium borohydride; In tetrahydrofuran; water; at 0 - 20 ℃; for 16.7h;
DOI:10.1021/ol4017518

Reference yield:

: 1448230-65-6
C₃₂H₆₇IO₄Si₂

: 1448230-77-0
C₅₁H₇₈O₁₀Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

1.2: 0.33 h / 20 °C

1.3: 13 h / 50 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

3.1: pyridinium p-toluenesulfonate / dichloromethane / 7.5 h / 0 - 20 °C

4.1: acetic acid / tetrahydrofuran; water / 16 h / 20 °C

5.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

6.2: 12 h / 0 - 20 °C

7.1: diisobutylaluminium hydride / dichloromethane; hexane / 2.25 h / -78 °C

8.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 2 h / 0 °C

9.1: triethylamine; di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 1 h / 0 °C

9.2: 2.25 h / -78 - 0 °C

9.3: 1 h / 0 °C

10.1: pyridine; silver nitrate / N,N-dimethyl-formamide / 1 h / 20 °C

11.1: lithium borohydride / tetrahydrofuran; water / 16.7 h / 0 - 20 °C

With pyridine; lithium borohydride; di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; tert.-butyl lithium; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; silver nitrate; acetic acid; triethylamine; 9-methoxy-9-BBN; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; pentane; 9.1: |Evans Aldol Reaction / 9.2: |Evans Aldol Reaction;
DOI:10.1021/ol4017518

Reference yield:

: C₂₂H₃₄O₄

: 1448230-77-0
C₅₁H₇₈O₁₀Si

Guidance literature:: Multi-step reaction with 16 steps

1.1: hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III); osmium(VIII) oxide; methanesulfonamide; potassium carbonate / water; tert-butyl alcohol / 23 h / 0 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.17 h / 20 °C / pH 7

4.1: triethylamine; dmap / dichloromethane / 25 h / 0 - 20 °C

5.1: sodium iodide / acetone / 18 h / 50 °C

6.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

6.2: 0.33 h / 20 °C

6.3: 13 h / 50 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

8.1: pyridinium p-toluenesulfonate / dichloromethane / 7.5 h / 0 - 20 °C

9.1: acetic acid / tetrahydrofuran; water / 16 h / 20 °C

10.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

11.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

11.2: 12 h / 0 - 20 °C

12.1: diisobutylaluminium hydride / dichloromethane; hexane / 2.25 h / -78 °C

13.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 2 h / 0 °C

14.1: triethylamine; di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 1 h / 0 °C

14.2: 2.25 h / -78 - 0 °C

14.3: 1 h / 0 °C

15.1: pyridine; silver nitrate / N,N-dimethyl-formamide / 1 h / 20 °C

16.1: lithium borohydride / tetrahydrofuran; water / 16.7 h / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; osmium(VIII) oxide; lithium borohydride; methanesulfonamide; di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; tert.-butyl lithium; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; silver nitrate; acetic acid; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; 9-methoxy-9-BBN; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; mineral oil; tert-butyl alcohol; pentane; 1.1: |Sharpless Dihydroxylation / 14.1: |Evans Aldol Reaction / 14.2: |Evans Aldol Reaction;
DOI:10.1021/ol4017518