(R)-N-((S)-3-allyl-6-bromo-2-oxo-1-tritylindolin-3-yl)-2-methylpropane-2-sulfinamide

Base Information

• Chemical Name: (R)-N-((S)-3-allyl-6-bromo-2-oxo-1-tritylindolin-3-yl)-2-methylpropane-2-sulfinamide
• CAS No.: 1422181-83-6
• Molecular Formula: C₃₄H₃₃BrN₂O₂S
• Molecular Weight: 613.618

Synonyms:(R)-N-((S)-3-allyl-6-bromo-2-oxo-1-tritylindolin-3-yl)-2-methylpropane-2-sulfinamide

Chemical Property of (R)-N-((S)-3-allyl-6-bromo-2-oxo-1-tritylindolin-3-yl)-2-methylpropane-2-sulfinamide

Chemical Property:

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Technology Process of (R)-N-((S)-3-allyl-6-bromo-2-oxo-1-tritylindolin-3-yl)-2-methylpropane-2-sulfinamide

There total 1 articles about (R)-N-((S)-3-allyl-6-bromo-2-oxo-1-tritylindolin-3-yl)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C31H27BrN2O2S + allyl bromide (106-95-6) → (R)-N-((S)-3-allyl-6-bromo-2-oxo-1-tritylindolin-3-yl)-2-methylpropane-2-sulfinamide (1422181-83-6)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; zinc; In tetrahydrofuran; at 20 ℃;

DOI:10.1039/c2cc38600c

Reference yield:

(R)-N-((S)-3-allyl-6-bromo-2-oxo-1-tritylindolin-3-yl)-2-methylpropane-2-sulfinamide (1422181-83-6) → C30H25BrN2O

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃;

DOI:10.1039/c2cc38600c

Reference yield:

(R)-N-((S)-3-allyl-6-bromo-2-oxo-1-tritylindolin-3-yl)-2-methylpropane-2-sulfinamide (1422181-83-6) → C32H27BrN2O2

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane / 20 °C

2: triethylamine / dichloromethane

With hydrogenchloride; triethylamine; In 1,4-dioxane; dichloromethane;

DOI:10.1039/c2cc38600c

upstream raw materials:

allyl bromide

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