butyl-methyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

Base Information

• Chemical Name: butyl-methyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester
• CAS No.: 1025963-39-6
• Molecular Formula: C₂₀H₃₂N₂O₄
• Molecular Weight: 364.485

Synonyms:butyl-methyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

Chemical Property of butyl-methyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

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Technology Process of butyl-methyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

There total 3 articles about butyl-methyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-n-butyl-N-methylcarbamoyl chloride (39214-35-2) + tert-butyl [(1R,S)-2-(3-hydroxyphenyl)-1-methylethyl]-carbamate (1027468-74-1) → butyl-methyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester (1025963-39-6)

Guidance literature:

With sodium hydride; In acetonitrile; at 20 ℃; for 6h;

DOI:10.1021/jm020120c

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → butyl-methyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester (1025963-39-6)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaHCO₃ / dioxane / 4 h / 20 °C

2: NaH / acetonitrile / 6 h / 20 °C

With sodium hydride; sodium hydrogencarbonate; In 1,4-dioxane; acetonitrile;

DOI:10.1021/jm020120c

Reference yield:

Desoxy metaraminol (1075-61-2,18840-47-6) → butyl-methyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester (1025963-39-6)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaHCO₃ / dioxane / 4 h / 20 °C

2: NaH / acetonitrile / 6 h / 20 °C

With sodium hydride; sodium hydrogencarbonate; In 1,4-dioxane; acetonitrile;

DOI:10.1021/jm020120c

upstream raw materials:

N-n-butyl-N-methylcarbamoyl chloride

tert-butyl [(1R,S)-2-(3-hydroxyphenyl)-1-methylethyl]-carbamate

di-tert-butyl dicarbonate

Desoxy metaraminol

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