1-(4-bromo-benzyl)-5-methyl-1H-[1,2,3]triazole-4-carbonyl chloride

Base Information

• Chemical Name: 1-(4-bromo-benzyl)-5-methyl-1H-[1,2,3]triazole-4-carbonyl chloride
• CAS No.: 952182-50-2
• Molecular Formula: C₁₁H₉BrClN₃O
• Molecular Weight: 314.569
• Mol file: 952182-50-2.mol

Synonyms:1-(4-bromo-benzyl)-5-methyl-1H-[1,2,3]triazole-4-carbonyl chloride

Chemical Property of 1-(4-bromo-benzyl)-5-methyl-1H-[1,2,3]triazole-4-carbonyl chloride

Chemical Property:

• Melting Point: 132°(dec)
• Boiling Point: 453.4±55.0 °C(Predicted)
• PKA: -1.63±0.10(Predicted)
• Density: 1?+-.0.1 g/cm3(Predicted)

Purity/Quality:

98%min ^*data from raw suppliers

1-(4-Bromobenzyl)-5-methyl-1H-1,2,3-triazole-4-carbonyl chloride >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(4-bromo-benzyl)-5-methyl-1H-[1,2,3]triazole-4-carbonyl chloride

There total 1 articles about 1-(4-bromo-benzyl)-5-methyl-1H-[1,2,3]triazole-4-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-(4-bromobenzyl)-5-methyl-1H-1,2,3-triazole-4-carboxylic acid (845885-94-1) → 1-(4-bromo-benzyl)-5-methyl-1H-[1,2,3]triazole-4-carbonyl chloride (952182-50-2)

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; for 1h;

Reference yield: 22.0%

1-(4-bromo-benzyl)-5-methyl-1H-[1,2,3]triazole-4-carbonyl chloride (952182-50-2) + 5-chloro-2-(1H-1,2,3,4-tetrazol-5-yl)aniline (54013-18-2) → 1-(4-bromo-benzyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid [5-chloro-2-(1H-tetrazol-5-yl)-phenyl]-amide (1083418-33-0)

Guidance literature:

With pyridine; In toluene;

upstream raw materials:

1-(4-bromobenzyl)-5-methyl-1H-1,2,3-triazole-4-carboxylic acid

Downstream raw materials:

1-(4-bromo-benzyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid [5-chloro-2-(1H-tetrazol-5-yl)-phenyl]-amide

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