4-tert-Butyl-3-phenyl-2,2-bis(trimethylsilyl)-1-[bis(trimethylsilyl)methylenephosphanyl]-1,2-dihydro-1,2-phosphasilete

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Chemical Name:4-tert-Butyl-3-phenyl-2,2-bis(trimethylsilyl)-1-[bis(trimethylsilyl)methylenephosphanyl]-1,2-dihydro-1,2-phosphasilete
CAS No.:129943-65-3
Molecular Formula:C₂₅H₅₀P₂Si₅
Molecular Weight:553.047
Hs Code.:

Synonyms:4-tert-Butyl-3-phenyl-2,2-bis(trimethylsilyl)-1-[bis(trimethylsilyl)methylenephosphanyl]-1,2-dihydro-1,2-phosphasilete

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Chemical Property of 4-tert-Butyl-3-phenyl-2,2-bis(trimethylsilyl)-1-[bis(trimethylsilyl)methylenephosphanyl]-1,2-dihydro-1,2-phosphasilete

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Technology Process of 4-tert-Butyl-3-phenyl-2,2-bis(trimethylsilyl)-1-[bis(trimethylsilyl)methylenephosphanyl]-1,2-dihydro-1,2-phosphasilete

There total 3 articles about 4-tert-Butyl-3-phenyl-2,2-bis(trimethylsilyl)-1-[bis(trimethylsilyl)methylenephosphanyl]-1,2-dihydro-1,2-phosphasilete which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 79454-85-6
[bis(trimethylsilyl)methylene]chlorophosphane

: 129943-64-2
4-tert-Butyl-3-phenyl-1,2,2-tris(trimethylsilyl)-1,2-dihydro-1,2-phosphasilete

: 129943-65-3
4-tert-Butyl-3-phenyl-2,2-bis(trimethylsilyl)-1-[bis(trimethylsilyl)methylenephosphanyl]-1,2-dihydro-1,2-phosphasilete

Guidance literature:: In diethyl ether; at 20 ℃; for 12h;
DOI:10.1002/(SICI)1521-3765(19990503)5:5<1581::AID-CHEM1581>3.0.CO;2-2

Reference yield:

: 129943-63-1
2-tert-butyl-3-phenyl-1-tris(trimethylsilyl)silyl-1H-phosphirene

: 129943-65-3
4-tert-Butyl-3-phenyl-2,2-bis(trimethylsilyl)-1-[bis(trimethylsilyl)methylenephosphanyl]-1,2-dihydro-1,2-phosphasilete

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / benzene / 40 h / 25 °C / Irradiation

2: 93 percent / diethyl ether / 12 h / 20 °C

In diethyl ether; benzene; 1: Isomerization / 2: Substitution;
DOI:10.1002/(SICI)1521-3765(19990503)5:5<1581::AID-CHEM1581>3.0.CO;2-2

Reference yield:

: 118398-71-3
1-chloro-3-(1,1-dimethylethyl)-2-phenyl-1H-phosphirene

: 129943-65-3
4-tert-Butyl-3-phenyl-2,2-bis(trimethylsilyl)-1-[bis(trimethylsilyl)methylenephosphanyl]-1,2-dihydro-1,2-phosphasilete

Guidance literature:: Multi-step reaction with 3 steps

1: pentane / -78 °C

2: 34 percent / benzene / 25 °C / Irradiation

3: 80 percent / diethyl ether / 25 °C

In diethyl ether; pentane; benzene;