3-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyloxy)-1-(4-isopropylphenyl)-5-(4-fluorophenyl)-1H-pyrazole

Base Information

Chemical Name:3-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyloxy)-1-(4-isopropylphenyl)-5-(4-fluorophenyl)-1H-pyrazole
CAS No.:1401696-32-9
Molecular Formula:C₃₂H₃₅FN₂O₁₀
Molecular Weight:626.636
Hs Code.:

Synonyms:3-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyloxy)-1-(4-isopropylphenyl)-5-(4-fluorophenyl)-1H-pyrazole

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Chemical Property of 3-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyloxy)-1-(4-isopropylphenyl)-5-(4-fluorophenyl)-1H-pyrazole

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Technology Process of 3-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyloxy)-1-(4-isopropylphenyl)-5-(4-fluorophenyl)-1H-pyrazole

There total 3 articles about 3-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyloxy)-1-(4-isopropylphenyl)-5-(4-fluorophenyl)-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1-(4-fluorophenyl)-5-(4-isopropylphenyl)-1H-pyrazol-3-ol

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1401696-32-9
3-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyloxy)-1-(4-isopropylphenyl)-5-(4-fluorophenyl)-1H-pyrazole

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In chloroform; water; at 55 ℃; for 4h; pH=8-10;
DOI:10.3390/molecules19011302

Reference yield: 46.0%

: 1246513-40-5
5-(4-fluorophenyl)-1-(4-isopropylphenyl)-1H-pyrazol-3-ol

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1401696-32-9
3-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyloxy)-1-(4-isopropylphenyl)-5-(4-fluorophenyl)-1H-pyrazole

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In chloroform; water; at 55 ℃; for 4h; pH=8 - 10;
DOI:10.1002/hlca.201100509

Reference yield:

: 3947-62-4
2,3,4,6-tetra-O-acetyl-β-D-glucopyranose

: 1401696-32-9
3-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyloxy)-1-(4-isopropylphenyl)-5-(4-fluorophenyl)-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide; acetic acid

2: tetrabutylammomium bromide; sodium hydroxide / chloroform; water / 4 h / 55 °C / pH 8 - 10

With tetrabutylammomium bromide; hydrogen bromide; acetic acid; sodium hydroxide; In chloroform; water;
DOI:10.1002/hlca.201100509